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<QUANDATASET description="" version="1"><XMLFILE filename="C:\Documents and Settings\Administrator\Desktop\5-31-13 Dewitt dosed male mice U2M3O-hexane high rerun samples.xml" modifieddate="31 May 2013" modifiedtime="14:40:05"/><DATASET filename="D:\Masslynx\new MJS.PRO\5-31-13 Dewitt dosed male mice U2M3O-hexane high rerun samples.qld" modifieddate="31 May 2013" modifiedtime="10:24:03" creationdate="31 May 2013" creationtime="10:24:03"/><GROUPDATA count="1"><GROUP id="1" name="5-31-13 U2M3O-HEX SERUM METHOD"><METHODDATA id="1" filename="D:\Masslynx\new MJS.PRO\MethDB\5-31-13 U2M3O-hex serum method.mdb" modifieddate="31 May 2013" modifiedtime="10:24:03" creationdate="30 May 2013" creationtime="14:32:16"/><SAMPLELISTDATA filename="D:\Masslynx\new MJS.PRO\SampleDB\5-31-13 redo of high dosed male mouse serum 100 mg_kg.SPL" modifieddate="31 May 2013" modifiedtime="07:53:27" count="24"><SAMPLE id="1" groupid="1" name="5-31-13 redo high Dewitt dose male mouse MB" createdate="31-May-13" createtime="08:02:16" type="Blank" text="Blank" desc="MB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="4" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="1" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="226.9917602539" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="189.5493774414" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="1290.8170000000" height="30356.0000000000" foundrt="0.6420000196" absresponse="1290.8170000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="1" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="1" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1290.8170000000" height="30356.0000000000" response="1290.8170000000" pkflags="bb" analconc="0.9987426043" empc="0.9987426043" bsanalconc="0.0000000000" conccalc="-0.1257395700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5835000277" endrt="0.7372000217" startht="91.4000015259" endht="346.0000000000" absresponse="1290.8170000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="50.2289810181" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1290.8170000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6322324428" pksigma="2.7630632415" pkskew="1.1248995731" pkkurt="2.4399144399" heightdivarea="23.5168889161" baselinewidth="9.2219996452" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="604.3522959202" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0369155444" peaktailwidth="0.0495086461" peakasymmetryvalue="1.3411327600"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="1" groupid="1"/></COMPOUND><USERDATA sampleid="1" groupid="1"/></SAMPLE><SAMPLE id="2" groupid="1" name="5-31-13 redo high Dewitt dose male mouse MtxB" createdate="31-May-13" createtime="08:04:37" type="Blank" text="Blank" desc="MtxB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="5" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="2" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="222.0188903809" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="189.8287963867" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="1406.8360000000" height="33878.0000000000" foundrt="0.6420000196" absresponse="1406.8360000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="2" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="2" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1406.8360000000" height="33878.0000000000" response="1406.8360000000" pkflags="bb" analconc="1.0885098744" empc="1.0885098744" bsanalconc="0.0000000000" conccalc="8.8509874400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="43.2000007629" endht="304.2000122070" absresponse="1406.8360000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="49.1162185669" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1406.8360000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6066404454" pksigma="2.5917330296" pkskew="1.1638772022" pkkurt="2.7462905750" heightdivarea="24.0809874072" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="689.7517966262" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0360752791" peaktailwidth="0.0464429222" peakasymmetryvalue="1.2873891592"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="2" groupid="1"/></COMPOUND><USERDATA sampleid="2" groupid="1"/></SAMPLE><SAMPLE id="3" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 1" createdate="31-May-13" createtime="08:06:58" type="Standard" text="Standard" desc="2500 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="6" stdconc="2500.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="3" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="2500.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="356.6570000000" height="9004.0000000000" response="0.4976727500" pkflags="bb" analconc="1630.3538423332" empc="1630.3538423332" bsanalconc="0.0000000000" conccalc="-34.7858463067" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6933000088" endrt="0.7957999706" startht="661.2000122070" endht="659.7999877930" absresponse="689.4390000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="178.7163391113" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0001990691" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5986192684" pksigma="2.6191512205" pkskew="0.4426350083" pkkurt="0.4363209769" heightdivarea="25.2455440381" baselinewidth="6.1499977112" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="50.3815154494" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0365044326" peaktailwidth="0.0381884910" peakasymmetryvalue="1.0461329222"><SECONDARYPEAK ion="1" foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="332.7820000000" height="7850.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8104000092" startht="609.2000122070" endht="738.7999877930" absresponse="0.0000000000" rrtref="0" ionratio="1.0716999769" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="231.8829345703" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6240629370" pksigma="3.4003990416" pkskew="0.6289531811" pkkurt="0.7462617689" heightdivarea="23.5890162328" baselinewidth="7.9020023346" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="33.8532890079" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0386831276" peaktailwidth="0.0466705747" peakasymmetryvalue="1.2064840794"/><ISPEAK area="1385.3260000000" height="33502.0000000000" foundrt="0.6420000196" absresponse="1385.3260000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="3" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="3" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1385.3260000000" height="33502.0000000000" response="1385.3260000000" pkflags="bb" analconc="1.0718669626" empc="1.0718669626" bsanalconc="0.0000000000" conccalc="7.1866962600" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="15.0000000000" endht="398.6000061035" absresponse="1385.3260000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="37.0431671143" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1385.3260000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6377881603" pksigma="2.5650297865" pkskew="1.1352928476" pkkurt="2.8747112577" heightdivarea="24.1834773909" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="904.4043101570" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0363060087" peaktailwidth="0.0446945466" peakasymmetryvalue="1.2310509682"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="3" groupid="1"/></COMPOUND><USERDATA sampleid="3" groupid="1"/></SAMPLE><SAMPLE id="4" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 2" createdate="31-May-13" createtime="08:09:19" type="Standard" text="Standard" desc="5000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="7" stdconc="5000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="4" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="5000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="6743.5360000000" height="160653.0000000000" response="10.3753210875" pkflags="bb" analconc="6917.3765161366" empc="6917.3765161366" bsanalconc="0.0000000000" conccalc="38.3475303227" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="778.4000244141" endht="2982.3999023438" absresponse="13373.5710000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="246.9871826172" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0020750642" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6278463661" pksigma="2.5423340132" pkskew="0.7579485870" pkkurt="1.1481911078" heightdivarea="23.8232583025" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="650.4507573942" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0374160893" peaktailwidth="0.0452352539" peakasymmetryvalue="1.2089786530"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="6630.0350000000" height="158405.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="895.5999755859" endht="2220.6000976563" absresponse="0.0000000000" rrtref="0" ionratio="1.0170999765" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="185.8534851074" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6202674395" pksigma="2.4999799984" pkskew="0.8032021524" pkkurt="1.3736036296" heightdivarea="23.8920307359" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="852.3111627874" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0364070423" peaktailwidth="0.0470345356" peakasymmetryvalue="1.2919076681"/><ISPEAK area="1288.9790000000" height="30779.0000000000" foundrt="0.6420000196" absresponse="1288.9790000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="4" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="4" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1288.9790000000" height="30779.0000000000" response="1288.9790000000" pkflags="bb" analconc="0.9973204903" empc="0.9973204903" bsanalconc="0.0000000000" conccalc="-0.2679509700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="27.6000003815" endht="204.8000030518" absresponse="1288.9790000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="55.9329528809" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1288.9790000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6155811711" pksigma="2.6166460450" pkskew="1.0813378099" pkkurt="2.2713389700" heightdivarea="23.8785891779" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="550.2838383227" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0364290401" peaktailwidth="0.0498923920" peakasymmetryvalue="1.3695774078"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="4" groupid="1"/></COMPOUND><USERDATA sampleid="4" groupid="1"/></SAMPLE><SAMPLE id="5" groupid="1" name="5-31-13 redo high Dewitt dose male mouse QC1" createdate="31-May-13" createtime="08:11:40" type="QC" text="QC" desc="5000 ng/mL QC" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="8" stdconc="5000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="5" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="5000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="5882.9720000000" height="139427.0000000000" response="8.5045848114" pkflags="bb" analconc="5900.5577363394" empc="5900.5577363394" bsanalconc="0.0000000000" conccalc="18.0111547268" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="729.4000244141" endht="2253.0000000000" absresponse="11447.8090000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="335.0303039551" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0017009170" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6094051327" pksigma="2.5060622811" pkskew="0.7798015717" pkkurt="1.2182621875" heightdivarea="23.7000958019" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="416.1623541335" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0377743170" peaktailwidth="0.0457410477" peakasymmetryvalue="1.2109034061"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="5564.8370000000" height="133718.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1228.8000488281" endht="2287.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0571999550" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="196.3755798340" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6109313873" pksigma="2.5651987659" pkskew="0.8355219698" pkkurt="1.4589282151" heightdivarea="24.0290955512" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="680.9298799425" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367502123" peaktailwidth="0.0462526865" peakasymmetryvalue="1.2585692406"/><ISPEAK area="1346.0750000000" height="31891.0000000000" foundrt="0.6420000196" absresponse="1346.0750000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="5" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="5" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1346.0750000000" height="31891.0000000000" response="1346.0750000000" pkflags="bb" analconc="1.0414973239" empc="1.0414973239" bsanalconc="0.0000000000" conccalc="4.1497323900" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="57.5999984741" endht="230.1999969482" absresponse="1346.0750000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="47.8744964600" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1346.0750000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6194510059" pksigma="2.6171592822" pkskew="1.0327010300" pkkurt="2.2176045534" heightdivarea="23.6918448081" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="666.1375546095" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0369708650" peaktailwidth="0.0486430153" peakasymmetryvalue="1.3157120943"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="5" groupid="1"/></COMPOUND><USERDATA sampleid="5" groupid="1"/></SAMPLE><SAMPLE id="6" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 3" createdate="31-May-13" createtime="08:14:00" type="Standard" text="Standard" desc="10000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="9" stdconc="10000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="6" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="10000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="11539.8780000000" height="268403.0000000000" response="17.0360393117" pkflags="bb" analconc="10600.5108113792" empc="10600.5108113792" bsanalconc="0.0000000000" conccalc="6.0051081138" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1155.8000488281" endht="4923.3999023438" absresponse="22161.9280000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="189.6709442139" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0017036039" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6233439770" pksigma="2.5626739989" pkskew="0.7805261388" pkkurt="1.1342037068" heightdivarea="23.2587380906" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1415.0981380541" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0394496992" peaktailwidth="0.0458018929" peakasymmetryvalue="1.1610201597"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="10622.0500000000" height="249930.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1185.5999755859" endht="3739.6000976563" absresponse="0.0000000000" rrtref="0" ionratio="1.0864000320" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="204.0641326904" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6339016123" pksigma="2.5726149054" pkskew="0.8075782680" pkkurt="1.2836935635" heightdivarea="23.5293563860" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1224.7620231192" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0372266285" peaktailwidth="0.0483961254" peakasymmetryvalue="1.3000406027"/><ISPEAK area="1300.8850000000" height="30959.0000000000" foundrt="0.6420000196" absresponse="1300.8850000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="6" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="6" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1300.8850000000" height="30959.0000000000" response="1300.8850000000" pkflags="bb" analconc="1.0065325084" empc="1.0065325084" bsanalconc="0.0000000000" conccalc="0.6532508400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="76.5999984741" endht="276.3999938965" absresponse="1300.8850000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="44.8018913269" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1300.8850000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6113734784" pksigma="2.7263122096" pkskew="1.2160817580" pkkurt="2.7257647900" heightdivarea="23.7984141565" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="691.0199342725" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367653668" peaktailwidth="0.0478326604" peakasymmetryvalue="1.3010250330"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="6" groupid="1"/></COMPOUND><USERDATA sampleid="6" groupid="1"/></SAMPLE><SAMPLE id="7" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 4" createdate="31-May-13" createtime="08:16:21" type="Standard" text="Standard" desc="15000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="10" stdconc="15000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="7" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="15000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="18284.7110000000" height="435202.0000000000" response="25.0464485244" pkflags="bb" analconc="15169.0465136040" empc="15169.0465136040" bsanalconc="0.0000000000" conccalc="1.1269767574" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1539.5999755859" endht="6621.2001953125" absresponse="35389.6800000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="238.7525329590" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0016697632" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6255011883" pksigma="2.4849361626" pkskew="0.7134674365" pkkurt="1.0782464356" heightdivarea="23.8014152917" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1822.8162633766" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0374126472" peaktailwidth="0.0447448753" peakasymmetryvalue="1.1959825754"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="17104.9690000000" height="401800.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1522.1999511719" endht="5048.7998046875" absresponse="0.0000000000" rrtref="0" ionratio="1.0690000057" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="243.6859130859" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6352701309" pksigma="2.5265552761" pkskew="0.7530136815" pkkurt="1.1524611929" heightdivarea="23.4902501139" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1648.8437715245" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0368458033" peaktailwidth="0.0482155941" peakasymmetryvalue="1.3085776567"/><ISPEAK area="1412.9620000000" height="34224.0000000000" foundrt="0.6420000196" absresponse="1412.9620000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="7" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="7" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1412.9620000000" height="34224.0000000000" response="1412.9620000000" pkflags="bb" analconc="1.0932497385" empc="1.0932497385" bsanalconc="0.0000000000" conccalc="9.3249738500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="11.0000000000" endht="276.2000122070" absresponse="1412.9620000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="62.3608016968" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1412.9620000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6044764938" pksigma="2.5678290117" pkskew="1.1042745235" pkkurt="2.6281724651" heightdivarea="24.2214581850" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="548.8062864620" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0364818648" peaktailwidth="0.0456922427" peakasymmetryvalue="1.2524645329"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="7" groupid="1"/></COMPOUND><USERDATA sampleid="7" groupid="1"/></SAMPLE><SAMPLE id="8" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 5" createdate="31-May-13" createtime="08:18:41" type="Standard" text="Standard" desc="20000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="11" stdconc="20000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="8" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="20000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="22645.1890000000" height="545297.0000000000" response="31.5708497112" pkflags="bb" analconc="19013.1209059382" empc="19013.1209059382" bsanalconc="0.0000000000" conccalc="-4.9343954703" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6933000088" endrt="0.8104000092" startht="2942.8000488281" endht="10383.7998046875" absresponse="43709.6520000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="209.9376983643" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0015785425" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6321511196" pksigma="2.5047041003" pkskew="0.7452310181" pkkurt="1.0574781053" heightdivarea="24.0800374861" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2597.4229699988" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370129719" peaktailwidth="0.0456113555" peakasymmetryvalue="1.2323071957"><SECONDARYPEAK ion="1" foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="21064.4630000000" height="493177.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="1837.1999511719" endht="7556.2001953125" absresponse="0.0000000000" rrtref="0" ionratio="1.0750000477" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="216.6748657227" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6354985646" pksigma="2.5032798779" pkskew="0.7521981658" pkkurt="1.1843332945" heightdivarea="23.4127497103" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2276.1154061647" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0397119373" peaktailwidth="0.0435455702" peakasymmetryvalue="1.0965360403"/><ISPEAK area="1384.4940000000" height="32940.0000000000" foundrt="0.6420000196" absresponse="1384.4940000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="8" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="8" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1384.4940000000" height="32940.0000000000" response="1384.4940000000" pkflags="bb" analconc="1.0712232201" empc="1.0712232201" bsanalconc="0.0000000000" conccalc="7.1223220100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5835000277" endrt="0.7372000217" startht="58.5999984741" endht="271.7999877930" absresponse="1384.4940000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="60.5161972046" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1384.4940000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6639209990" pksigma="2.5348512003" pkskew="1.0208597142" pkkurt="2.4610374026" heightdivarea="23.7920857729" baselinewidth="9.2219996452" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="544.3170840467" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0352153257" peaktailwidth="0.0463956967" peakasymmetryvalue="1.3174859285"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="8" groupid="1"/></COMPOUND><USERDATA sampleid="8" groupid="1"/></SAMPLE><SAMPLE id="9" groupid="1" name="5-31-13 redo high Dewitt dose male mouse DB004" createdate="31-May-13" createtime="08:21:02" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="12" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="9" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="220.3895263672" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="221.9372253418" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="9" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="9" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="43.3148422241" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="9" groupid="1"/></COMPOUND><USERDATA sampleid="9" groupid="1"/></SAMPLE><SAMPLE id="10" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 1" createdate="31-May-13" createtime="08:23:22" type="Analyte" text="Analyte" desc="M-21-100 11-6" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="13" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="10" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="25884.8810000000" height="598175.0000000000" response="41.3938387606" pkflags="bb" analconc="25034.1494401140" empc="25034.1494401140" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="3849.0000000000" endht="10829.0000000000" absresponse="50407.0160000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="200.7640991211" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6412213429" pksigma="2.6056787118" pkskew="0.7445818708" pkkurt="1.1131297437" heightdivarea="23.1090496418" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2979.4918644254" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0369038694" peaktailwidth="0.0499222353" peakasymmetryvalue="1.3527642488"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="24522.1350000000" height="570511.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4555.3999023438" endht="7013.3999023438" absresponse="0.0000000000" rrtref="0" ionratio="1.0556000471" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="194.2864990234" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6420332354" pksigma="2.6235745195" pkskew="0.8010901319" pkkurt="1.2011323472" heightdivarea="23.2651439200" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2936.4418159142" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0374974385" peaktailwidth="0.0492204316" peakasymmetryvalue="1.3126345873"/><ISPEAK area="1217.7420000000" height="29139.0000000000" foundrt="0.6420000196" absresponse="1217.7420000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="10" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="10" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1217.7420000000" height="29139.0000000000" response="1217.7420000000" pkflags="bb" analconc="0.9422023544" empc="0.9422023544" bsanalconc="0.0000000000" conccalc="-5.7797645600" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="74.0000000000" endht="230.3999938965" absresponse="1217.7420000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="50.9406394958" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1217.7420000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6414359043" pksigma="2.6289267490" pkskew="1.1685600885" pkkurt="2.7540935289" heightdivarea="23.9287139640" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="572.0187317706" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0369746424" peaktailwidth="0.0448385514" peakasymmetryvalue="1.2126837969"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="10" groupid="1"/></COMPOUND><USERDATA sampleid="10" groupid="1"/></SAMPLE><SAMPLE id="11" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 2" createdate="31-May-13" createtime="08:25:42" type="Analyte" text="Analyte" desc="M-22-100 11-6" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="14" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="11" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="27519.6050000000" height="651230.0000000000" response="41.4487917469" pkflags="bb" analconc="25068.6883152489" empc="25068.6883152489" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6933000088" endrt="0.8104000092" startht="4743.7998046875" endht="11135.7998046875" absresponse="53227.2120000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="278.8081665039" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6435094856" pksigma="2.5445395682" pkskew="0.7511169123" pkkurt="0.9986973630" heightdivarea="23.6642204712" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2335.7637194278" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0372240394" peaktailwidth="0.0473541170" peakasymmetryvalue="1.2721381187"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="25707.6070000000" height="599091.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4519.3999023438" endht="8606.7998046875" absresponse="0.0000000000" rrtref="0" ionratio="1.0705000162" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="181.3795013428" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6353168971" pksigma="2.5617609898" pkskew="0.7538020832" pkkurt="1.1365661210" heightdivarea="23.3040360388" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3302.9697157885" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0365176313" peaktailwidth="0.0495414734" peakasymmetryvalue="1.3566452265"/><ISPEAK area="1284.1680000000" height="30545.0000000000" foundrt="0.6420000196" absresponse="1284.1680000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="11" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="11" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1284.1680000000" height="30545.0000000000" response="1284.1680000000" pkflags="bb" analconc="0.9935980799" empc="0.9935980799" bsanalconc="0.0000000000" conccalc="-0.6401920100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="88.4000015259" endht="308.6000061035" absresponse="1284.1680000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="59.1672973633" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1284.1680000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6188587924" pksigma="2.6455295931" pkskew="1.1082179901" pkkurt="2.4871066352" heightdivarea="23.7858286455" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="516.2480180978" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0366623998" peaktailwidth="0.0476935655" peakasymmetryvalue="1.3008849621"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="11" groupid="1"/></COMPOUND><USERDATA sampleid="11" groupid="1"/></SAMPLE><SAMPLE id="12" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 3" createdate="31-May-13" createtime="08:28:03" type="Analyte" text="Analyte" desc="M-19-100 11-10" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="15" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="12" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="28005.4120000000" height="659116.0000000000" response="39.0997618678" pkflags="bb" analconc="23601.1022540424" empc="23601.1022540424" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6933000088" endrt="0.8104000092" startht="6461.0000000000" endht="10417.5996093750" absresponse="53953.9960000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="208.0918121338" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6241579976" pksigma="2.5368983395" pkskew="0.7393370673" pkkurt="1.0376609314" heightdivarea="23.5353081040" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3167.4288057823" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0383046716" peaktailwidth="0.0460935235" peakasymmetryvalue="1.2033394575"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="25948.5840000000" height="608339.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4094.0000000000" endht="8172.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0793000460" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="173.5348205566" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6450803491" pksigma="2.5636448043" pkskew="0.7670024902" pkkurt="1.1974186402" heightdivarea="23.4440152881" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3505.5731065884" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0371006429" peaktailwidth="0.0483239107" peakasymmetryvalue="1.3025087118"/><ISPEAK area="1379.9060000000" height="33250.0000000000" foundrt="0.6420000196" absresponse="1379.9060000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="12" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="12" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1379.9060000000" height="33250.0000000000" response="1379.9060000000" pkflags="bb" analconc="1.0676733512" empc="1.0676733512" bsanalconc="0.0000000000" conccalc="6.7673351200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5759999752" endrt="0.7372000217" startht="50.0000000000" endht="420.7999877930" absresponse="1379.9060000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="39.8593482971" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1379.9060000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6051987695" pksigma="2.6858473841" pkskew="1.1286266610" pkkurt="2.7878492977" heightdivarea="24.0958442097" baselinewidth="9.6720027924" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="834.1832323035" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0364727899" peaktailwidth="0.0468278751" peakasymmetryvalue="1.2839126587"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="12" groupid="1"/></COMPOUND><USERDATA sampleid="12" groupid="1"/></SAMPLE><SAMPLE id="13" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 6" createdate="31-May-13" createtime="08:30:25" type="Standard" text="Standard" desc="25000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="16" stdconc="25000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="13" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="25000.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="28546.4300000000" height="667593.0000000000" response="39.5568409370" pkflags="bb" analconc="23885.2664973440" empc="23885.2664973440" bsanalconc="0.0000000000" conccalc="-4.4589340106" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="2201.8000488281" endht="11780.5996093750" absresponse="53711.5840000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="285.1544799805" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0015822736" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6288956144" pksigma="2.5495866613" pkskew="0.7440810455" pkkurt="1.0559176004" heightdivarea="23.3862167704" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2341.1625868397" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0384353362" peaktailwidth="0.0458629318" peakasymmetryvalue="1.1932491064"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="25165.1540000000" height="584715.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="2370.3999023438" endht="8377.2001953125" absresponse="0.0000000000" rrtref="0" ionratio="1.1344000101" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="261.3135681152" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6337205120" pksigma="2.5715004836" pkskew="0.7633546144" pkkurt="1.1642715649" heightdivarea="23.2351051776" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2237.5990815071" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0371686444" peaktailwidth="0.0494132154" peakasymmetryvalue="1.3294327259"/><ISPEAK area="1357.8330000000" height="33015.0000000000" foundrt="0.6420000196" absresponse="1357.8330000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="13" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="13" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1357.8330000000" height="33015.0000000000" response="1357.8330000000" pkflags="bb" analconc="1.0505948300" empc="1.0505948300" bsanalconc="0.0000000000" conccalc="5.0594830000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="65.8000030518" endht="188.0000000000" absresponse="1357.8330000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="63.4457359314" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1357.8330000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5945083535" pksigma="2.5449856642" pkskew="1.0735559243" pkkurt="2.4607640816" heightdivarea="24.3144775536" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="520.3659397331" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0362542383" peaktailwidth="0.0480508171" peakasymmetryvalue="1.3253848553"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="13" groupid="1"/></COMPOUND><USERDATA sampleid="13" groupid="1"/></SAMPLE><SAMPLE id="14" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 4" createdate="31-May-13" createtime="08:32:45" type="Analyte" text="Analyte" desc="M-21-100 11-10" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="17" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="14" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="30722.6500000000" height="706882.0000000000" response="44.9685789310" pkflags="bb" analconc="27302.1744924277" empc="27302.1744924277" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="5204.6000976563" endht="12109.0000000000" absresponse="59613.5410000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="316.3235778809" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6409500732" pksigma="2.6117278757" pkskew="0.7297527795" pkkurt="0.9607048854" heightdivarea="23.0084969884" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2234.6800852962" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0396010540" peaktailwidth="0.0477877855" peakasymmetryvalue="1.2067302465"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="28890.8910000000" height="667824.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4570.6000976563" endht="9389.4003906250" absresponse="0.0000000000" rrtref="0" ionratio="1.0634000301" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="249.3275756836" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6439683275" pksigma="2.6259811914" pkskew="0.7813166762" pkkurt="1.1268009393" heightdivarea="23.1153826305" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2678.5003550810" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0372985266" peaktailwidth="0.0493752547" peakasymmetryvalue="1.3237856627"/><ISPEAK area="1325.6710000000" height="31650.0000000000" foundrt="0.6420000196" absresponse="1325.6710000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="14" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="14" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1325.6710000000" height="31650.0000000000" response="1325.6710000000" pkflags="bb" analconc="1.0257101565" empc="1.0257101565" bsanalconc="0.0000000000" conccalc="2.5710156500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="39.4000015259" endht="148.0000000000" absresponse="1325.6710000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="48.5430107117" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1325.6710000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6300078355" pksigma="2.5293652838" pkskew="1.0287049353" pkkurt="2.1122511191" heightdivarea="23.8747019434" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="651.9991145170" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0363289602" peaktailwidth="0.0481384695" peakasymmetryvalue="1.3250715733"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="14" groupid="1"/></COMPOUND><USERDATA sampleid="14" groupid="1"/></SAMPLE><SAMPLE id="15" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 5" createdate="31-May-13" createtime="08:35:06" type="Analyte" text="Analyte" desc="M-22-100 11-10" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="18" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="15" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="27427.1580000000" height="645670.0000000000" response="41.1846946441" pkflags="bb" analconc="24902.7902271249" empc="24902.7902271248" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6933000088" endrt="0.8104000092" startht="5113.3999023438" endht="11692.7998046875" absresponse="53888.4020000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="236.0612182617" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6271270746" pksigma="2.5557640049" pkskew="0.7389300391" pkkurt="1.0095986097" heightdivarea="23.5412651942" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2735.1803263345" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0377424955" peaktailwidth="0.0473356172" peakasymmetryvalue="1.2541729212"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="26461.2440000000" height="617614.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4417.6000976563" endht="9257.7998046875" absresponse="0.0000000000" rrtref="0" ionratio="1.0364999771" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="248.7520751953" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6574202700" pksigma="2.5864324258" pkskew="0.7769418027" pkkurt="1.1765786925" heightdivarea="23.3403236824" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2482.8496386013" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0368824303" peaktailwidth="0.0489065386" peakasymmetryvalue="1.3260117769"/><ISPEAK area="1308.4570000000" height="31827.0000000000" foundrt="0.6420000196" absresponse="1308.4570000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="15" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="15" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1308.4570000000" height="31827.0000000000" response="1308.4570000000" pkflags="bb" analconc="1.0123911847" empc="1.0123911847" bsanalconc="0.0000000000" conccalc="1.2391184700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5982000232" endrt="0.7372000217" startht="47.5999984741" endht="408.3999938965" absresponse="1308.4570000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="43.7326736450" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1308.4570000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5782411063" pksigma="2.6296492758" pkskew="1.2172767576" pkkurt="2.9551353357" heightdivarea="24.3240702599" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="727.7625022047" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0365589112" peaktailwidth="0.0462743118" peakasymmetryvalue="1.2657464743"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="15" groupid="1"/></COMPOUND><USERDATA sampleid="15" groupid="1"/></SAMPLE><SAMPLE id="16" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 6" createdate="31-May-13" createtime="08:37:27" type="Analyte" text="Analyte" desc="M-22-100 11-19" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="19" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="16" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="29004.7270000000" height="673284.0000000000" response="48.3089692499" pkflags="bb" analconc="29461.9938129082" empc="29461.9938129082" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4450.0000000000" endht="10385.5996093750" absresponse="55714.5410000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="275.8583068848" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6411462299" pksigma="2.5830844656" pkskew="0.7747419523" pkkurt="1.1265199398" heightdivarea="23.2129059515" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2440.6877849839" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0365922190" peaktailwidth="0.0500609279" peakasymmetryvalue="1.3680757284"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="26709.8140000000" height="625789.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4701.0000000000" endht="8173.2001953125" absresponse="0.0000000000" rrtref="0" ionratio="1.0858999491" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="240.2064971924" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6208224215" pksigma="2.6152360822" pkskew="0.8249189186" pkkurt="1.2487772153" heightdivarea="23.4291785035" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2605.2126287775" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0372748524" peaktailwidth="0.0497485511" peakasymmetryvalue="1.3346410990"/><ISPEAK area="1153.2960000000" height="27250.0000000000" foundrt="0.6420000196" absresponse="1153.2960000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="16" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="16" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1153.2960000000" height="27250.0000000000" response="1153.2960000000" pkflags="bb" analconc="0.8923386124" empc="0.8923386124" bsanalconc="0.0000000000" conccalc="-10.7661387600" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="33.4000015259" endht="242.6000061035" absresponse="1153.2960000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="47.1713447571" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1153.2960000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6149920966" pksigma="2.7232497896" pkskew="1.1939825492" pkkurt="2.6529007704" heightdivarea="23.6279324649" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="577.6812202478" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0373867489" peaktailwidth="0.0483120084" peakasymmetryvalue="1.2922227383"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="16" groupid="1"/></COMPOUND><USERDATA sampleid="16" groupid="1"/></SAMPLE><SAMPLE id="17" groupid="1" name="5-31-13 redo high Dewitt dose male mouse sample 7" createdate="31-May-13" createtime="08:39:48" type="Analyte" text="Analyte" desc="M-23-100 11-19" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="20" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="17" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="40293.5510000000" height="940242.0000000000" response="57.1158455605" pkflags="bb" analconc="35361.4073694643" empc="35361.4073694643" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="5609.7998046875" endht="14488.4003906250" absresponse="75218.3130000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="235.5130310059" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6382771698" pksigma="2.6115041371" pkskew="0.7905795201" pkkurt="1.1574477380" heightdivarea="23.3348011447" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3992.3141236996" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0369061381" peaktailwidth="0.0505249873" peakasymmetryvalue="1.3690131903"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="34924.7620000000" height="799537.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="6408.0000000000" endht="11673.5996093750" absresponse="0.0000000000" rrtref="0" ionratio="1.1536999941" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="242.2395172119" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6445463602" pksigma="2.6803489131" pkskew="0.8136599054" pkkurt="1.1969188366" heightdivarea="22.8931266590" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3300.6051580781" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0383361094" peaktailwidth="0.0502098761" peakasymmetryvalue="1.3097280264"/><ISPEAK area="1316.9430000000" height="31818.0000000000" foundrt="0.6420000196" absresponse="1316.9430000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="17" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="17" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1316.9430000000" height="31818.0000000000" response="1316.9430000000" pkflags="bb" analconc="1.0189570494" empc="1.0189570494" bsanalconc="0.0000000000" conccalc="1.8957049400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7225000262" startht="20.0000000000" endht="223.3999938965" absresponse="1316.9430000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="48.4645385742" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1316.9430000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6062427709" pksigma="2.4169952120" pkskew="0.8674708829" pkkurt="1.6144759832" heightdivarea="24.1604989738" baselinewidth="7.9080033302" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="656.5212614430" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367363021" peaktailwidth="0.0457537957" peakasymmetryvalue="1.2454655170"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="17" groupid="1"/></COMPOUND><USERDATA sampleid="17" groupid="1"/></SAMPLE><SAMPLE id="18" groupid="1" name="5-31-13 redo high Dewitt dose male mouse DB005" createdate="31-May-13" createtime="08:42:09" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="21" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="18" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="239.9705505371" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="228.3432922363" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="18" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="18" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="50.0788421631" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="18" groupid="1"/></COMPOUND><USERDATA sampleid="18" groupid="1"/></SAMPLE><SAMPLE id="19" groupid="1" name="5-31-13 redo high Dewitt dose male mouse QC2" createdate="31-May-13" createtime="08:44:29" type="QC" text="QC" desc="5000 ng/mL QC" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="22" stdconc="5000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="19" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="5000.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="5361.0680000000" height="125640.0000000000" response="9.1791299899" pkflags="bb" analconc="6266.3360497755" empc="6266.3360497755" bsanalconc="0.0000000000" conccalc="25.3267209955" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="866.5999755859" endht="2303.1999511719" absresponse="10514.5190000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="284.8526306152" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0018358260" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6720997508" pksigma="2.5942500235" pkskew="0.7865054619" pkkurt="1.2087330287" heightdivarea="23.4356288710" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="441.0701762825" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367537439" peaktailwidth="0.0483916737" peakasymmetryvalue="1.3166460991"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="5153.4510000000" height="121301.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8104000092" startht="991.0000000000" endht="1473.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0403000116" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="185.9390869141" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6309352680" pksigma="2.6030437967" pkskew="0.8440974886" pkkurt="1.5187172246" heightdivarea="23.5378196086" baselinewidth="7.9020023346" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="652.3695582955" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0372539014" peaktailwidth="0.0482279845" peakasymmetryvalue="1.2945754528"/><ISPEAK area="1145.4810000000" height="27158.0000000000" foundrt="0.6420000196" absresponse="1145.4810000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="19" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="19" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1145.4810000000" height="27158.0000000000" response="1145.4810000000" pkflags="bb" analconc="0.8862919199" empc="0.8862919199" bsanalconc="0.0000000000" conccalc="-11.3708080100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="26.2000007629" endht="262.7999877930" absresponse="1145.4810000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="40.4015388489" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1145.4810000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6245159941" pksigma="2.6892248713" pkskew="1.2587993914" pkkurt="3.0990864669" heightdivarea="23.7088175186" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="672.2021183793" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0378311649" peaktailwidth="0.0433787964" peakasymmetryvalue="1.1466418505"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="19" groupid="1"/></COMPOUND><USERDATA sampleid="19" groupid="1"/></SAMPLE><SAMPLE id="20" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 7" createdate="31-May-13" createtime="08:46:50" type="Standard" text="Standard" desc="30000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="23" stdconc="30000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="20" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="30000.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="29252.1370000000" height="673622.0000000000" response="47.8224192878" pkflags="bb" analconc="29144.8811805195" empc="29144.8811805195" bsanalconc="0.0000000000" conccalc="-2.8503960649" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="2117.0000000000" endht="10653.0000000000" absresponse="56526.5300000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="252.3370513916" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0015940806" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6347045832" pksigma="2.6087351562" pkskew="0.7807343420" pkkurt="1.0975671806" heightdivarea="23.0281295346" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2669.5326599288" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370859168" peaktailwidth="0.0507665873" peakasymmetryvalue="1.3688912392"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="27274.3930000000" height="629752.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8104000092" startht="2380.3999023438" endht="8552.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0724999905" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="265.3654785156" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6362656153" pksigma="2.6468143015" pkskew="0.7918124015" pkkurt="1.2003931084" heightdivarea="23.0894964372" baselinewidth="7.9020023346" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2373.1496784082" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0376737453" peaktailwidth="0.0500275306" peakasymmetryvalue="1.3279149532"/><ISPEAK area="1182.0090000000" height="28051.0000000000" foundrt="0.6420000196" absresponse="1182.0090000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="20" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="20" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1182.0090000000" height="28051.0000000000" response="1182.0090000000" pkflags="bb" analconc="0.9145546944" empc="0.9145546944" bsanalconc="0.0000000000" conccalc="-8.5445305600" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5835000277" endrt="0.7372000217" startht="96.8000030518" endht="160.3999938965" absresponse="1182.0090000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="53.6226043701" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1182.0090000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5819931387" pksigma="2.6436359538" pkskew="1.0251292650" pkkurt="2.2443573133" heightdivarea="23.7316297930" baselinewidth="9.2219996452" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="523.1189407807" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367856361" peaktailwidth="0.0512075759" peakasymmetryvalue="1.3920536041"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="20" groupid="1"/></COMPOUND><USERDATA sampleid="20" groupid="1"/></SAMPLE><SAMPLE id="21" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 8" createdate="31-May-13" createtime="08:49:10" type="Standard" text="Standard" desc="40000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="24" stdconc="40000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="21" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="40000.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="39359.7150000000" height="900738.0000000000" response="62.3172326076" pkflags="bb" analconc="39000.7733674972" empc="39000.7733674972" bsanalconc="0.0000000000" conccalc="-2.4980665813" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="3024.3999023438" endht="16398.1992187500" absresponse="75502.3750000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="254.5564575195" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0015579308" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6781992782" pksigma="2.6168178249" pkskew="0.7684871329" pkkurt="1.0615969724" heightdivarea="22.8847693638" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3538.4606180375" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0367320329" peaktailwidth="0.0515603051" peakasymmetryvalue="1.4036877155"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="36142.6600000000" height="843976.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="3479.6000976563" endht="12400.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0889999866" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="263.5585937500" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6512968491" pksigma="2.6237095810" pkskew="0.8366156780" pkkurt="1.2949745600" heightdivarea="23.3512419949" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3202.2329000608" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0373605676" peaktailwidth="0.0492076501" peakasymmetryvalue="1.3171013594"/><ISPEAK area="1211.5810000000" height="29215.0000000000" foundrt="0.6420000196" absresponse="1211.5810000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="21" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="21" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1211.5810000000" height="29215.0000000000" response="1211.5810000000" pkflags="bb" analconc="0.9374354097" empc="0.9374354097" bsanalconc="0.0000000000" conccalc="-6.2564590300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7300000191" startht="70.5999984741" endht="141.1999969482" absresponse="1211.5810000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="54.4943161011" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1211.5810000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6123209273" pksigma="2.5565684533" pkskew="1.0103666129" pkkurt="2.0720149467" heightdivarea="24.1131216155" baselinewidth="8.3580029011" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="536.1109578073" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0366539136" peaktailwidth="0.0473121032" peakasymmetryvalue="1.2907789946"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="21" groupid="1"/></COMPOUND><USERDATA sampleid="21" groupid="1"/></SAMPLE><SAMPLE id="22" groupid="1" name="5-31-13 redo high Dewitt dose male mouse std 9" createdate="31-May-13" createtime="08:51:30" type="Standard" text="Standard" desc="50000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="25" stdconc="50000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="22" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="50000.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="45622.7190000000" height="1045366.0000000000" response="79.8413020913" pkflags="bb" analconc="52316.0372428888" empc="52316.0372428888" bsanalconc="0.0000000000" conccalc="4.6320744858" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8104000092" startht="4227.7998046875" endht="19155.4003906250" absresponse="88456.9770000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="331.1566162109" detectionthreshold="1369.1489945768" detectionflag="0" quanthreshold="1369.1489945768" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0015968260" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6418220305" pksigma="2.6475361409" pkskew="0.7973525148" pkkurt="1.1148754911" heightdivarea="22.9132770451" baselinewidth="7.4700021744" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3156.7118059152" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370740891" peaktailwidth="0.0516644903" peakasymmetryvalue="1.3935471773"><SECONDARYPEAK ion="1" foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="42834.2580000000" height="980361.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8104000092" startht="3468.6000976563" endht="14133.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0650999546" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="230.0508728027" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6303217631" pksigma="2.6749882660" pkskew="0.8180323055" pkkurt="1.2077732219" heightdivarea="22.8873113665" baselinewidth="7.9020023346" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="4261.4965466384" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379387103" peaktailwidth="0.0501224995" peakasymmetryvalue="1.3211439848"/><ISPEAK area="1107.9100000000" height="26544.0000000000" foundrt="0.6420000196" absresponse="1107.9100000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="22" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="22" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="74" foundrt="0.6420000196" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="1107.9100000000" height="26544.0000000000" response="1107.9100000000" pkflags="bb" analconc="0.8572221459" empc="0.8572221459" bsanalconc="0.0000000000" conccalc="-14.2777854100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.5906999707" endrt="0.7372000217" startht="58.5999984741" endht="150.3999938965" absresponse="1107.9100000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="43.8555526733" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="1107.9100000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5978679225" pksigma="2.6118241071" pkskew="1.1916571102" pkkurt="2.7582193148" heightdivarea="23.9586247980" baselinewidth="8.7900030613" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="605.2597306825" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0366621539" peaktailwidth="0.0488686487" peakasymmetryvalue="1.3329453468"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="22" groupid="1"/></COMPOUND><USERDATA sampleid="22" groupid="1"/></SAMPLE><SAMPLE id="23" groupid="1" name="5-31-13 redo high Dewitt dose male mouse DB end 001" createdate="31-May-13" createtime="08:53:50" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="26" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="23" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="247.1243286133" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="251.9187927246" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="23" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="23" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="48.3958129883" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="23" groupid="1"/></COMPOUND><USERDATA sampleid="23" groupid="1"/></SAMPLE><SAMPLE id="24" groupid="1" name="5-31-13 redo high Dewitt dose male mouse DB end 002" createdate="31-May-13" createtime="08:56:11" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="10.0000000000" job="5-31-13 redo of high dosed male mouse serum 100 mg" sampleid="" samplenumber="27" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="24" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="230.2666168213" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7300000191" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="228.6833038330" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7300000191" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="24" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="24" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="45.5598869324" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.6449999809" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="24" groupid="1"/></COMPOUND><USERDATA sampleid="24" groupid="1"/></SAMPLE></SAMPLELISTDATA><CALIBRATIONDATA filename="" modifieddate="31 May 2013" modifiedtime="10:24:03" count="2"><COMPOUND id="1" name="U2M3O-hex"><RESPONSE type="Internal Std" ref="2" rah="Area * ( IS Conc. / IS Area )"/><CURVE type="2nd Order" origin="Exclude" weighting="1/x" axistrans="None"><CALIBRATIONCURVE curve="-0.000000 * x^2 + 0.001925 * x + -2.623527"/><DETERMINATION rsquared="0.9862546962"/></CURVE></COMPOUND><COMPOUND id="2" name="13C-PFHxA"><RESPONSE type="External Std" ref="" rah="Area"/><CURVE type="RF" origin="" weighting="" axistrans=""><RESPONSEFACTOR cc="1292.4421111111" stddev="105.3395378603" percrelsd="8.1504260001"/></CURVE></COMPOUND></CALIBRATIONDATA></GROUP></GROUPDATA></QUANDATASET>
