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<QUANDATASET description="" version="1"><XMLFILE filename="C:\Documents and Settings\Administrator\Desktop\5-29-13 redo Dewitt male mouse U2M3O-hexane 0 and 1 mg_kg.xml" modifieddate="31 May 2013" modifiedtime="14:41:32"/><DATASET filename="D:\Masslynx\new MJS.PRO\5-29-13 redo Dewitt male mouse U2M3O-hexane 0 and 1 mg_kg.qld" modifieddate="30 May 2013" modifiedtime="10:40:59" creationdate="30 May 2013" creationtime="10:12:34"/><GROUPDATA count="1"><GROUP id="1" name="4-22-13 U2M3O-HEX SERUM METHOD"><METHODDATA id="1" filename="D:\Masslynx\new MJS.PRO\MethDB\4-22-13 U2M3O-hex serum method.mdb" modifieddate="30 May 2013" modifiedtime="10:12:33" creationdate="28 May 2013" creationtime="16:15:01"/><SAMPLELISTDATA filename="D:\Masslynx\new MJS.PRO\SampleDB\5-28-13 redo Dewitt dosed male mouse serum U2M3O-hexane 0 and 1 mk_kg.SPL" modifieddate="29 May 2013" modifiedtime="14:03:51" count="61"><SAMPLE id="1" groupid="1" name="5-29-13 redo Dewitt dose male mouse MB" createdate="29-May-13" createtime="16:40:11" type="Blank" text="Blank" desc="MB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="4" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="1" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="316.2630310059" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="224.0469818115" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4383.2490000000" height="99413.0000000000" foundrt="0.7225000262" absresponse="4383.2490000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="1" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="1" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4383.2490000000" height="99413.0000000000" response="4383.2490000000" pkflags="bb" analconc="1.0764377497" empc="1.0760000000" bsanalconc="0.0000000000" conccalc="7.6437749700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8616999984" startht="14.4000000000" endht="444.0000000000" absresponse="4383.2490000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="67.1517639160" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4383.2490000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6150000000" pksigma="3.2680000000" pkskew="1.7290000000" pkkurt="4.7950000000" heightdivarea="22.6802082200" baselinewidth="12.2999989986" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1480.4227648336" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6629999876"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="1" groupid="1"/></COMPOUND><USERDATA sampleid="1" groupid="1"/></SAMPLE><SAMPLE id="2" groupid="1" name="5-29-13 redo Dewitt dose male mouse MtxB" createdate="29-May-13" createtime="16:42:49" type="Blank" text="Blank" desc="MtxB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="5" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="2" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="289.4546508789" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="314.8821411133" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4496.8130000000" height="104024.0000000000" foundrt="0.7300000191" absresponse="4496.8130000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="2" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="2" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4496.8130000000" height="104024.0000000000" response="4496.8130000000" pkflags="bb" analconc="1.1043267828" empc="1.1040000000" bsanalconc="0.0000000000" conccalc="10.4326782800" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8616999984" startht="51.2000000000" endht="377.8000000000" absresponse="4496.8130000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="56.8200454712" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4496.8130000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6090000000" pksigma="3.0880000000" pkskew="1.6640000000" pkkurt="4.5470000000" heightdivarea="23.1328276270" baselinewidth="10.9800016880" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1830.7623504585" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5429999828"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="2" groupid="1"/></COMPOUND><USERDATA sampleid="2" groupid="1"/></SAMPLE><SAMPLE id="3" groupid="1" name="5-29-13 redo Dewitt dose male mouse std1" createdate="29-May-13" createtime="16:45:28" type="Standard" text="Standard" desc="10 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="6" stdconc="10.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="3" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="10.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="157.6050000000" height="3778.0000000000" response="0.0588788851" pkflags="bb" analconc="6.0092394486" empc="6.0090000000" bsanalconc="0.0000000000" conccalc="-39.9076055140" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8690000176" startht="1094.8000000000" endht="1377.8000000000" absresponse="263.9720000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="277.1654968262" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0058878885" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5870000000" pksigma="3.6040000000" pkskew="0.5230000000" pkkurt="-0.5630000000" heightdivarea="23.9713207068" baselinewidth="6.1440002918" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="13.6308452649" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0520000011" peakasymmetryvalue="1.4589999914"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="106.3670000000" height="2807.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8398000002" startht="1371.6000000000" endht="1441.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.4816999435" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="276.7773132324" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="1.9250000000" pksigma="2.6500000000" pkskew="0.2540000000" pkkurt="-0.7210000000" heightdivarea="26.3897637425" baselinewidth="4.3919992447" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="10.1417271785" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0320000015" peakasymmetryvalue="0.9070000052"/><ISPEAK area="4483.3050000000" height="98562.0000000000" foundrt="0.7225000262" absresponse="4483.3050000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="3" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="3" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4483.3050000000" height="98562.0000000000" response="4483.3050000000" pkflags="bb" analconc="1.1010094899" empc="1.1010000000" bsanalconc="0.0000000000" conccalc="10.1009489900" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8837000132" startht="56.0000000000" endht="164.0000000000" absresponse="4483.3050000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="83.4133148193" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4483.3050000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6340000000" pksigma="3.5090000000" pkskew="1.8090000000" pkkurt="5.1550000000" heightdivarea="21.9842281531" baselinewidth="13.1820023060" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1181.6099169956" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0649999976" peakasymmetryvalue="1.7079999447"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="3" groupid="1"/></COMPOUND><USERDATA sampleid="3" groupid="1"/></SAMPLE><SAMPLE id="4" groupid="1" name="5-29-13 redo Dewitt dose male mouse std2" createdate="29-May-13" createtime="16:48:06" type="Standard" text="Standard" desc="25 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="7" stdconc="25.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="4" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="25.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="260.6370000000" height="6372.0000000000" response="0.1153688155" pkflags="bb" analconc="25.0802161824" empc="25.0800000000" bsanalconc="0.0000000000" conccalc="0.3208647296" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8763999939" startht="1238.8000000000" endht="1468.0000000000" absresponse="530.2270000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="257.7500305176" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0046147526" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5930000000" pksigma="3.7570000000" pkskew="0.6620000000" pkkurt="-0.1110000000" heightdivarea="24.4477952094" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="24.7216265589" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0489999987" peakasymmetryvalue="1.3780000210"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="269.5900000000" height="6316.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7300000191" endrt="0.8690000176" startht="1020.8000000000" endht="1434.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.9667999744" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="296.6905517578" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6430000000" pksigma="4.1280000000" pkskew="0.1350000000" pkkurt="0.0280000000" heightdivarea="23.4281687006" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="21.2881736967" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0410000011" peaktailwidth="0.0469999984" peakasymmetryvalue="1.1519999504"/><ISPEAK area="4595.9300000000" height="101890.0000000000" foundrt="0.7225000262" absresponse="4595.9300000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="4" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="4" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4595.9300000000" height="101890.0000000000" response="4595.9300000000" pkflags="bb" analconc="1.1286679235" empc="1.1290000000" bsanalconc="0.0000000000" conccalc="12.8667923500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8471000195" startht="36.4000000000" endht="607.8000000000" absresponse="4595.9300000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="67.7411346436" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4595.9300000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6430000000" pksigma="3.3050000000" pkskew="1.5350000000" pkkurt="3.5430000000" heightdivarea="22.1696152901" baselinewidth="10.9860026836" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1504.1082576507" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7029999495"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="4" groupid="1"/></COMPOUND><USERDATA sampleid="4" groupid="1"/></SAMPLE><SAMPLE id="5" groupid="1" name="5-29-13 redo Dewitt dose male mouse std3" createdate="29-May-13" createtime="16:50:45" type="Standard" text="Standard" desc="50 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="8" stdconc="50.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="5" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="50.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="456.2440000000" height="11479.0000000000" response="0.1989162110" pkflags="bb" analconc="53.3477059140" empc="53.3480000000" bsanalconc="0.0000000000" conccalc="6.6954118280" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1417.6000000000" endht="1541.8000000000" absresponse="864.5730000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="391.3349609375" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0039783242" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6420000000" pksigma="3.6860000000" pkskew="0.8080000000" pkkurt="0.7170000000" heightdivarea="25.1597829232" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="29.3329274044" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0740000010"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="408.3290000000" height="9897.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8616999984" startht="1236.4000000000" endht="1328.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1173000336" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="271.1934204102" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5990000000" pksigma="2.9970000000" pkskew="0.6810000000" pkkurt="0.2420000000" heightdivarea="24.2378082380" baselinewidth="6.1559987068" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="36.4942482197" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0469999984" peakasymmetryvalue="1.3409999609"/><ISPEAK area="4346.4180000000" height="95863.0000000000" foundrt="0.7225000262" absresponse="4346.4180000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="5" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="5" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4346.4180000000" height="95863.0000000000" response="4346.4180000000" pkflags="bb" analconc="1.0673927972" empc="1.0670000000" bsanalconc="0.0000000000" conccalc="6.7392797200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8616999984" startht="67.8000000000" endht="205.4000000000" absresponse="4346.4180000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="59.4588012695" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4346.4180000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6160000000" pksigma="3.3520000000" pkskew="1.6300000000" pkkurt="4.0960000000" heightdivarea="22.0556329373" baselinewidth="11.4179992676" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1612.2592106330" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7189999819"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="5" groupid="1"/></COMPOUND><USERDATA sampleid="5" groupid="1"/></SAMPLE><SAMPLE id="6" groupid="1" name="5-29-13 redo Dewitt dose male mouse std4" createdate="29-May-13" createtime="16:53:24" type="Standard" text="Standard" desc="100 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="9" stdconc="100.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="6" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="100.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="876.1490000000" height="22031.0000000000" response="0.3706922510" pkflags="bb" analconc="111.7009644612" empc="111.7010000000" bsanalconc="0.0000000000" conccalc="11.7009644612" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8763999939" startht="1339.2000000000" endht="1753.8000000000" absresponse="1670.5250000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="330.8172912598" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0037069225" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6060000000" pksigma="2.9550000000" pkskew="1.0480000000" pkkurt="1.2100000000" heightdivarea="25.1452663873" baselinewidth="6.5879988670" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="66.5956725421" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1679999828"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="794.3760000000" height="19021.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7372000217" endrt="0.8690000176" startht="1295.2000000000" endht="1485.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1029000282" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="306.2990112305" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6360000000" pksigma="3.2020000000" pkskew="0.3570000000" pkkurt="0.8390000000" heightdivarea="23.9445804002" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="62.0994495659" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0430000015" peakasymmetryvalue="1.1549999714"/><ISPEAK area="4506.5010000000" height="99989.0000000000" foundrt="0.7225000262" absresponse="4506.5010000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="6" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="6" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4506.5010000000" height="99989.0000000000" response="4506.5010000000" pkflags="bb" analconc="1.1067059607" empc="1.1070000000" bsanalconc="0.0000000000" conccalc="10.6705960700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8471000195" startht="161.4000000000" endht="665.4000000000" absresponse="4506.5010000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="63.9259872437" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4506.5010000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6160000000" pksigma="3.2720000000" pkskew="1.4800000000" pkkurt="3.2950000000" heightdivarea="22.1877239126" baselinewidth="10.1040029526" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1564.1369701323" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0649999976" peakasymmetryvalue="1.7530000210"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="6" groupid="1"/></COMPOUND><USERDATA sampleid="6" groupid="1"/></SAMPLE><SAMPLE id="7" groupid="1" name="5-29-13 redo Dewitt dose male mouse std5" createdate="29-May-13" createtime="16:56:03" type="Standard" text="Standard" desc="250 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="10" stdconc="250.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="7" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="250.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="1746.6080000000" height="45214.0000000000" response="0.7616380128" pkflags="bb" analconc="245.7077033411" empc="245.7080000000" bsanalconc="0.0000000000" conccalc="-1.7169186636" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8763999939" startht="2166.0000000000" endht="2048.8000000000" absresponse="3425.2240000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="294.5493469238" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0030465521" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5940000000" pksigma="2.6510000000" pkskew="1.1090000000" pkkurt="1.9270000000" heightdivarea="25.8867473411" baselinewidth="6.5879988670" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="153.5022924756" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0359999985" peakasymmetryvalue="1.0140000582"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="1678.6160000000" height="41386.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1379.8000000000" endht="1784.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0405000448" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="249.3191528320" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6060000000" pksigma="2.9280000000" pkskew="1.2940000000" pkkurt="2.4290000000" heightdivarea="24.6548346972" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="165.9960718216" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0340000018" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2549999952"/><ISPEAK area="4497.1810000000" height="100269.0000000000" foundrt="0.7225000262" absresponse="4497.1810000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="7" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="7" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4497.1810000000" height="100269.0000000000" response="4497.1810000000" pkflags="bb" analconc="1.1044171562" empc="1.1040000000" bsanalconc="0.0000000000" conccalc="10.4417156200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8690000176" startht="51.2000000000" endht="419.6000000000" absresponse="4497.1810000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="74.0794677734" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4497.1810000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6110000000" pksigma="3.3850000000" pkskew="1.7950000000" pkkurt="5.1220000000" heightdivarea="22.2959671848" baselinewidth="11.8560004234" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1353.5329425781" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0619999990" peakasymmetryvalue="1.6579999924"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="7" groupid="1"/></COMPOUND><USERDATA sampleid="7" groupid="1"/></SAMPLE><SAMPLE id="8" groupid="1" name="5-29-13 redo Dewitt dose male mouse std6" createdate="29-May-13" createtime="16:58:43" type="Standard" text="Standard" desc="500 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="11" stdconc="500.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="8" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="500.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="3233.0810000000" height="80613.0000000000" response="1.4826467893" pkflags="bb" analconc="497.4137240107" empc="497.4140000000" bsanalconc="0.0000000000" conccalc="-0.5172551979" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1340.6000000000" endht="2152.6000000000" absresponse="6397.6120000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="319.2488708496" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0029652936" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6040000000" pksigma="2.6790000000" pkskew="1.0800000000" pkkurt="2.2820000000" heightdivarea="24.9338015348" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="252.5083324037" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1480000019"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="3164.5310000000" height="78517.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7080000043" endrt="0.8690000176" startht="1180.0000000000" endht="1921.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0217000246" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="336.6336364746" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5990000000" pksigma="2.7350000000" pkskew="-0.1040000000" pkkurt="3.0530000000" heightdivarea="24.8115755542" baselinewidth="9.6600008011" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="233.2416951029" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0329999998" peaktailwidth="0.0410000011" peakasymmetryvalue="1.2269999981"/><ISPEAK area="4314.9940000000" height="94853.0000000000" foundrt="0.7225000262" absresponse="4314.9940000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="8" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="8" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4314.9940000000" height="94853.0000000000" response="4314.9940000000" pkflags="bb" analconc="1.0596756952" empc="1.0600000000" bsanalconc="0.0000000000" conccalc="5.9675695200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8544999957" startht="55.6000000000" endht="216.4000000000" absresponse="4314.9940000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="63.0055503845" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4314.9940000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6090000000" pksigma="3.3180000000" pkskew="1.5430000000" pkkurt="3.5430000000" heightdivarea="21.9821858385" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1505.4705406288" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7239999771"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="8" groupid="1"/></COMPOUND><USERDATA sampleid="8" groupid="1"/></SAMPLE><SAMPLE id="9" groupid="1" name="5-29-13 redo Dewitt dose male mouse std7" createdate="29-May-13" createtime="17:01:22" type="Standard" text="Standard" desc="1000 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="12" stdconc="1000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="9" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="1000.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5713.3900000000" height="142883.0000000000" response="2.3581437660" pkflags="bb" analconc="811.5582764125" empc="811.5580000000" bsanalconc="0.0000000000" conccalc="-18.8441723588" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8763999939" startht="1904.8000000000" endht="2474.8000000000" absresponse="10915.8640000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="316.7749938965" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0023581438" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6140000000" pksigma="2.4280000000" pkskew="0.8670000000" pkkurt="1.5470000000" heightdivarea="25.0084450738" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="451.0551740290" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1269999743"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5202.4740000000" height="128776.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8837000132" startht="1923.2000000000" endht="2188.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0981999636" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="350.1410827637" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6050000000" pksigma="2.5830000000" pkskew="0.9960000000" pkkurt="2.4980000000" heightdivarea="24.7528387456" baselinewidth="8.3460009098" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="367.7831775225" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1749999523"/><ISPEAK area="4629.0070000000" height="102726.0000000000" foundrt="0.7225000262" absresponse="4629.0070000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="9" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="9" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4629.0070000000" height="102726.0000000000" response="4629.0070000000" pkflags="bb" analconc="1.1367909691" empc="1.1370000000" bsanalconc="0.0000000000" conccalc="13.6790969100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8544999957" startht="35.0000000000" endht="485.4000000000" absresponse="4629.0070000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="83.0427627563" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4629.0070000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6290000000" pksigma="3.2730000000" pkskew="1.6130000000" pkkurt="4.1390000000" heightdivarea="22.1918005309" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1237.0253179245" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0619999990" peakasymmetryvalue="1.6499999762"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="9" groupid="1"/></COMPOUND><USERDATA sampleid="9" groupid="1"/></SAMPLE><SAMPLE id="10" groupid="1" name="5-29-13 redo Dewitt dose male mouse std8" createdate="29-May-13" createtime="17:04:01" type="Standard" text="Standard" desc="2500 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="13" stdconc="2500.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="10" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="2500.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="14144.2660000000" height="354855.0000000000" response="6.3683952172" pkflags="bb" analconc="2398.9795969258" empc="2398.9800000000" bsanalconc="0.0000000000" conccalc="-4.0408161230" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="2151.4000000000" endht="2861.2000000000" absresponse="26582.8980000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="278.4860839844" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0025473581" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6130000000" pksigma="2.3480000000" pkskew="0.8630000000" pkkurt="1.7200000000" heightdivarea="25.0882583798" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1274.2288408921" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1299999952"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="12438.6320000000" height="309709.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="2184.6000000000" endht="2842.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1370999813" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="345.0568237305" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6290000000" pksigma="2.3230000000" pkskew="0.8080000000" pkkurt="1.5840000000" heightdivarea="24.8989599499" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="897.5594125387" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1870000362"/><ISPEAK area="4174.1910000000" height="91205.0000000000" foundrt="0.7225000262" absresponse="4174.1910000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="10" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="10" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4174.1910000000" height="91205.0000000000" response="4174.1910000000" pkflags="bb" analconc="1.0250973118" empc="1.0250000000" bsanalconc="0.0000000000" conccalc="2.5097311800" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8544999957" startht="26.4000000000" endht="566.0000000000" absresponse="4174.1910000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="79.1676177979" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4174.1910000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6400000000" pksigma="3.3670000000" pkskew="1.5620000000" pkkurt="3.8380000000" heightdivarea="21.8497428604" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1152.0493168417" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7100000381"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="10" groupid="1"/></COMPOUND><USERDATA sampleid="10" groupid="1"/></SAMPLE><SAMPLE id="11" groupid="1" name="5-29-13 redo Dewitt dose male mouse DB004" createdate="29-May-13" createtime="17:06:40" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="14" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="11" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="343.7951965332" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="310.2729187012" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="11" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="11" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="53.2736587524" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="11" groupid="1"/></COMPOUND><USERDATA sampleid="11" groupid="1"/></SAMPLE><SAMPLE id="12" groupid="1" name="5-29-13 redo Dewitt dose male mouse QCL" createdate="29-May-13" createtime="17:09:18" type="QC" text="QC" desc="100 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="15" stdconc="100.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="12" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="100.0000000000"><PEAK foundscan="97" foundrt="0.8104000092" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="647.2440000000" height="16826.0000000000" response="0.3191682597" pkflags="bb" analconc="94.1646531224" empc="94.1650000000" bsanalconc="0.0000000000" conccalc="-5.8353468776" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7738000154" endrt="0.8837000132" startht="1154.8000000000" endht="1607.0000000000" absresponse="1250.7320000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="263.8050537109" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0031916826" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5750000000" pksigma="3.0360000000" pkskew="1.0820000000" pkkurt="1.2120000000" heightdivarea="25.9963784910" baselinewidth="6.5939998627" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="63.7819471739" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0350000001" peakasymmetryvalue="0.9869999886"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="603.4880000000" height="15398.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8616999984" startht="1332.6000000000" endht="1326.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0724999905" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="288.8565063477" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="2.5400000000" pkskew="0.5870000000" pkkurt="0.4480000000" heightdivarea="25.5150060979" baselinewidth="5.7059991360" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="53.3067445656" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0329999998" peaktailwidth="0.0390000008" peakasymmetryvalue="1.1929999590"/><ISPEAK area="3918.7230000000" height="89971.0000000000" foundrt="0.7372000217" absresponse="3918.7230000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="12" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="12" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="87" foundrt="0.7372000217" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3918.7230000000" height="89971.0000000000" response="3918.7230000000" pkflags="bb" analconc="0.9623595118" empc="0.9620000000" bsanalconc="0.0000000000" conccalc="-3.7640488200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6858999729" endrt="0.8544999957" startht="72.2000000000" endht="623.2000000000" absresponse="3918.7230000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="68.1858978271" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3918.7230000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6120000000" pksigma="3.0360000000" pkskew="1.4540000000" pkkurt="3.3940000000" heightdivarea="22.9592650463" baselinewidth="10.1160013676" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1319.4957149069" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0599999987" peakasymmetryvalue="1.6280000210"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="12" groupid="1"/></COMPOUND><USERDATA sampleid="12" groupid="1"/></SAMPLE><SAMPLE id="13" groupid="1" name="5-29-13 redo Dewitt dose male mouse QCH" createdate="29-May-13" createtime="17:11:56" type="QC" text="QC" desc="1000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="16" stdconc="1000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="13" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="1000.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5301.6410000000" height="134448.0000000000" response="2.3997348490" pkflags="bb" analconc="826.7276302466" empc="826.7280000000" bsanalconc="0.0000000000" conccalc="-17.3272369753" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8763999939" startht="1617.2000000000" endht="2704.4000000000" absresponse="9935.5790000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="256.4508056641" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0023997348" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6080000000" pksigma="2.4040000000" pkskew="0.8870000000" pkkurt="1.6640000000" heightdivarea="25.3596952340" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="524.2642917493" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0399999991" peakasymmetryvalue="1.1150000095"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="4633.9380000000" height="113180.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1731.6000000000" endht="1425.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1440999508" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="306.7790527344" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="2.4850000000" pkskew="1.0070000000" pkkurt="2.1340000000" heightdivarea="24.4241506900" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="368.9300132822" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1130000353"/><ISPEAK area="4140.2820000000" height="92533.0000000000" foundrt="0.7225000262" absresponse="4140.2820000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="13" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="13" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4140.2820000000" height="92533.0000000000" response="4140.2820000000" pkflags="bb" analconc="1.0167699437" empc="1.0170000000" bsanalconc="0.0000000000" conccalc="1.6769943700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8616999984" startht="65.6000000000" endht="481.2000000000" absresponse="4140.2820000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="68.2320938110" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4140.2820000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6440000000" pksigma="3.3770000000" pkskew="1.6790000000" pkkurt="4.2850000000" heightdivarea="22.3494438302" baselinewidth="11.4179992676" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1356.1506738495" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0649999976" peakasymmetryvalue="1.7589999437"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="13" groupid="1"/></COMPOUND><USERDATA sampleid="13" groupid="1"/></SAMPLE><SAMPLE id="14" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 1" createdate="29-May-13" createtime="17:14:35" type="Analyte" text="Analyte" desc="M1 0 mg/kg 11/6/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="17" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="14" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="471.6910000000" height="12061.0000000000" response="0.1858851732" pkflags="bb" analconc="48.9338916824" empc="48.9340000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8690000176" startht="1520.6000000000" endht="1652.8000000000" absresponse="924.7700000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="274.0561218262" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5960000000" pksigma="3.1040000000" pkskew="0.8450000000" pkkurt="0.3990000000" heightdivarea="25.5697055912" baselinewidth="6.1440002918" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="44.0092340198" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0390000008" peakasymmetryvalue="1.0829999447"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="453.0790000000" height="11541.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="1344.8000000000" endht="1495.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0411000252" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="298.6942138672" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="3.5260000000" pkskew="0.8890000000" pkkurt="0.7350000000" heightdivarea="25.4723789891" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="38.6381773205" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1820000410"/><ISPEAK area="4974.9530000000" height="111250.0000000000" foundrt="0.7225000262" absresponse="4974.9530000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="14" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="14" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4974.9530000000" height="111250.0000000000" response="4974.9530000000" pkflags="bb" analconc="1.2217483452" empc="1.2220000000" bsanalconc="0.0000000000" conccalc="22.1748345200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8471000195" startht="101.4000000000" endht="855.4000000000" absresponse="4974.9530000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="71.0650024414" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4974.9530000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6210000000" pksigma="3.3120000000" pkskew="1.6010000000" pkkurt="3.9130000000" heightdivarea="22.3620203045" baselinewidth="10.5420005322" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1565.4681795266" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6030000448"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="14" groupid="1"/></COMPOUND><USERDATA sampleid="14" groupid="1"/></SAMPLE><SAMPLE id="15" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 2" createdate="29-May-13" createtime="17:17:14" type="Analyte" text="Analyte" desc="M4  0 mg/kg 11/6/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="18" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="15" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="97" foundrt="0.8104000092" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="39.5750000000" height="1126.0000000000" response="0.0206419981" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:13:18" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8324000239" startht="1283.8000000000" endht="1732.4000000000" absresponse="91.5530000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="243.9053344727" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5930000000" pksigma="2.8280000000" pkskew="-0.1630000000" pkkurt="-0.8680000000" heightdivarea="28.4523057486" baselinewidth="4.3980002403" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="4.6165451954" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0149999997" peakasymmetryvalue="0.4149999917"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="51.9780000000" height="1200.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8544999957" startht="1184.0000000000" endht="1383.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.7613999844" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="265.4142150879" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5940000000" pksigma="3.6510000000" pkskew="0.0910000000" pkkurt="-0.9570000000" heightdivarea="23.0866905229" baselinewidth="5.7239985466" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="4.5212348540" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0399999991" peaktailwidth="0.0410000011" peakasymmetryvalue="1.0049999952"/><ISPEAK area="4435.2780000000" height="98568.0000000000" foundrt="0.7225000262" absresponse="4435.2780000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="15" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="15" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4435.2780000000" height="98568.0000000000" response="4435.2780000000" pkflags="bb" analconc="1.0892150251" empc="1.0890000000" bsanalconc="0.0000000000" conccalc="8.9215025100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8616999984" startht="72.0000000000" endht="405.8000000000" absresponse="4435.2780000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="62.1900558472" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4435.2780000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6030000000" pksigma="3.3610000000" pkskew="1.6660000000" pkkurt="4.3400000000" heightdivarea="22.2236351363" baselinewidth="11.8620014191" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1584.9479254727" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7020000219"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="15" groupid="1"/></COMPOUND><USERDATA sampleid="15" groupid="1"/></SAMPLE><SAMPLE id="16" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 3" createdate="29-May-13" createtime="17:19:52" type="Analyte" text="Analyte" desc="M5 0 mg/kg 11/6/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="19" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="16" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="97" foundrt="0.8104000092" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="44.8890000000" height="823.0000000000" response="0.0099621855" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:40:42" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7153000236" endrt="0.8251000047" startht="723.4000000000" endht="1814.6000000000" absresponse="44.8890000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="249.2800903320" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.9060000000" pksigma="4.1480000000" pkskew="-0.4410000000" pkkurt="-0.8070000000" heightdivarea="18.3341130344" baselinewidth="6.5879988670" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3.3015071477" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0790000036" peaktailwidth="0.0130000003" peakasymmetryvalue="0.1630000025"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="329.9407348633" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4505.9390000000" height="100789.0000000000" foundrt="0.7300000191" absresponse="4505.9390000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="16" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="16" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4505.9390000000" height="100789.0000000000" response="4505.9390000000" pkflags="bb" analconc="1.1065679448" empc="1.1070000000" bsanalconc="0.0000000000" conccalc="10.6567944800" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8763999939" startht="53.4000000000" endht="285.6000000000" absresponse="4505.9390000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="69.4629898071" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4505.9390000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6180000000" pksigma="3.3390000000" pkskew="1.7330000000" pkkurt="4.7630000000" heightdivarea="22.3680347204" baselinewidth="12.2999989986" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1450.9741126872" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7339999676"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="16" groupid="1"/></COMPOUND><USERDATA sampleid="16" groupid="1"/></SAMPLE><SAMPLE id="17" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 4" createdate="29-May-13" createtime="17:22:30" type="Analyte" text="Analyte" desc="M7 1 mg/kg 11/6/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="20" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="17" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="7164.3130000000" height="179581.0000000000" response="3.4375373152" pkflags="bb" analconc="1212.9934885504" empc="1212.9930000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="2297.6000000000" endht="1780.4000000000" absresponse="14042.8040000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="253.7447509766" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6040000000" pksigma="2.3840000000" pkskew="0.9310000000" pkkurt="1.9260000000" heightdivarea="25.0660461094" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="707.7230142057" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1519999504"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="6878.4910000000" height="170082.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="2446.4000000000" endht="1954.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0415999889" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="270.3477783203" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6170000000" pksigma="2.4230000000" pkskew="1.0070000000" pkkurt="2.2620000000" heightdivarea="24.7266442596" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="629.1229802469" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0329999998" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2949999571"/><ISPEAK area="4085.1350000000" height="91014.0000000000" foundrt="0.7225000262" absresponse="4085.1350000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="17" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="17" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4085.1350000000" height="91014.0000000000" response="4085.1350000000" pkflags="bb" analconc="1.0032269503" empc="1.0030000000" bsanalconc="0.0000000000" conccalc="0.3226950300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8690000176" startht="57.8000000000" endht="378.4000000000" absresponse="4085.1350000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="45.8008499146" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4085.1350000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6740000000" pksigma="3.3540000000" pkskew="1.7540000000" pkkurt="5.0160000000" heightdivarea="22.2793126788" baselinewidth="11.8560004234" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1987.1683641199" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0649999976" peakasymmetryvalue="1.7369999886"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="17" groupid="1"/></COMPOUND><USERDATA sampleid="17" groupid="1"/></SAMPLE><SAMPLE id="18" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 5" createdate="29-May-13" createtime="17:25:09" type="Analyte" text="Analyte" desc="M10 1 mg/kg 11/6/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="21" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="18" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5011.0030000000" height="127532.0000000000" response="2.1274885040" pkflags="bb" analconc="727.8461150643" empc="727.8460000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8763999939" startht="1988.4000000000" endht="2178.6000000000" absresponse="9768.0720000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="275.8151855469" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6060000000" pksigma="2.3160000000" pkskew="0.8700000000" pkkurt="1.6130000000" heightdivarea="25.4503938633" baselinewidth="6.5879988670" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="462.3820829413" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0390000008" peakasymmetryvalue="1.1200000048"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="4757.0690000000" height="121014.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1815.6000000000" endht="1709.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0534000397" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="331.6060180664" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="2.3940000000" pkskew="1.0360000000" pkkurt="2.4960000000" heightdivarea="25.4387733287" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="364.9330633552" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0590000153"/><ISPEAK area="4591.3630000000" height="106889.0000000000" foundrt="0.7300000191" absresponse="4591.3630000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="18" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="18" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4591.3630000000" height="106889.0000000000" response="4591.3630000000" pkflags="bb" analconc="1.1275463602" empc="1.1280000000" bsanalconc="0.0000000000" conccalc="12.7546360200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8471000195" startht="81.8000000000" endht="739.0000000000" absresponse="4591.3630000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="60.5872039795" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4591.3630000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6150000000" pksigma="3.0590000000" pkskew="1.5360000000" pkkurt="3.8110000000" heightdivarea="23.2804507071" baselinewidth="10.1040029526" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1764.2174086162" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5269999504"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="18" groupid="1"/></COMPOUND><USERDATA sampleid="18" groupid="1"/></SAMPLE><SAMPLE id="19" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 6" createdate="29-May-13" createtime="17:27:47" type="Analyte" text="Analyte" desc="M1 0 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="22" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="19" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="449.8980000000" height="11723.0000000000" response="0.1785777252" pkflags="bb" analconc="46.4595372485" empc="46.4600000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8837000132" startht="1286.8000000000" endht="1303.4000000000" absresponse="834.6230000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="352.7092285156" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5980000000" pksigma="3.3440000000" pkskew="1.0800000000" pkkurt="1.1040000000" heightdivarea="26.0570173684" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="33.2370095598" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0340000018" peakasymmetryvalue="0.9829999804"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="384.7250000000" height="9844.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8544999957" startht="1164.6000000000" endht="1176.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1693999767" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="300.6530761719" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5950000000" pksigma="2.6640000000" pkskew="0.4600000000" pkkurt="0.1800000000" heightdivarea="25.5871076743" baselinewidth="5.7239985466" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="32.7420564770" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0350000001" peakasymmetryvalue="0.9789999723"/><ISPEAK area="4673.7240000000" height="106121.0000000000" foundrt="0.7300000191" absresponse="4673.7240000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="19" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="19" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4673.7240000000" height="106121.0000000000" response="4673.7240000000" pkflags="bb" analconc="1.1477725644" empc="1.1480000000" bsanalconc="0.0000000000" conccalc="14.7772564400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8763999939" startht="47.8000000000" endht="487.0000000000" absresponse="4673.7240000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="47.1632804871" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4673.7240000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6120000000" pksigma="3.4010000000" pkskew="1.8130000000" pkkurt="5.0730000000" heightdivarea="22.7058765130" baselinewidth="12.2999989986" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2250.0767313910" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7330000401"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="19" groupid="1"/></COMPOUND><USERDATA sampleid="19" groupid="1"/></SAMPLE><SAMPLE id="20" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 7" createdate="29-May-13" createtime="17:30:27" type="Analyte" text="Analyte" desc="M3 0 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="23" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="20" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="638.4550000000" height="15988.0000000000" response="0.2646143054" pkflags="MM" analconc="75.6282820636" empc="75.6280000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:13:35" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8690000176" startht="1245.8310000000" endht="1245.8310000000" absresponse="1199.5800000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="323.5322875977" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6040000000" pksigma="3.1010000000" pkskew="0.6480000000" pkkurt="0.9580000000" heightdivarea="25.0417022343" baselinewidth="7.4640011787" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="49.4170152807" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0329999998" peaktailwidth="0.0469999984" peakasymmetryvalue="1.4320000410"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="561.1250000000" height="13831.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8544999957" startht="1222.8000000000" endht="1291.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1377999783" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="221.1846923828" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.7220000000" pksigma="2.7840000000" pkskew="0.5120000000" pkkurt="0.2600000000" heightdivarea="24.6486968144" baselinewidth="6.1559987068" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="62.5314521136" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0430000015" peakasymmetryvalue="1.1740000248"/><ISPEAK area="4533.3150000000" height="99967.0000000000" foundrt="0.7153000236" absresponse="4533.3150000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="20" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="20" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4533.3150000000" height="99967.0000000000" response="4533.3150000000" pkflags="bb" analconc="1.1132909395" empc="1.1130000000" bsanalconc="0.0000000000" conccalc="11.3290939500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8471000195" startht="42.8000000000" endht="580.2000000000" absresponse="4533.3150000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="60.2040023804" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4533.3150000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6160000000" pksigma="3.3110000000" pkskew="1.5640000000" pkkurt="3.8170000000" heightdivarea="22.0516332970" baselinewidth="10.9860026836" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1660.4709993931" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0630000010" peakasymmetryvalue="1.6890000105"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="20" groupid="1"/></COMPOUND><USERDATA sampleid="20" groupid="1"/></SAMPLE><SAMPLE id="21" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 8" createdate="29-May-13" createtime="17:33:05" type="Analyte" text="Analyte" desc="M4 0 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="24" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="21" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="253.3110000000" height="6340.0000000000" response="0.1090638701" pkflags="bb" analconc="22.9499992749" empc="22.9500000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7372000217" endrt="0.8471000195" startht="993.8000000000" endht="1306.8000000000" absresponse="489.9690000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="272.5416259766" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5880000000" pksigma="3.2380000000" pkskew="-0.4510000000" pkkurt="0.1810000000" heightdivarea="25.0285222513" baselinewidth="6.5939998627" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="23.2625015620" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0500000007" peaktailwidth="0.0340000018" peakasymmetryvalue="0.6819999814"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="236.6580000000" height="6182.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8544999957" startht="885.8000000000" endht="1355.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0703999996" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="267.0148925781" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5970000000" pksigma="2.7790000000" pkskew="0.5270000000" pkkurt="-0.1820000000" heightdivarea="26.1220833439" baselinewidth="5.2739989758" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="23.1522666781" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0350000001" peakasymmetryvalue="0.9860000014"/><ISPEAK area="4492.4960000000" height="104724.0000000000" foundrt="0.7300000191" absresponse="4492.4960000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="21" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="21" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4492.4960000000" height="104724.0000000000" response="4492.4960000000" pkflags="bb" analconc="1.1032666145" empc="1.1030000000" bsanalconc="0.0000000000" conccalc="10.3266614500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8544999957" startht="53.6000000000" endht="469.8000000000" absresponse="4492.4960000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="91.7559051514" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4492.4960000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6110000000" pksigma="3.0490000000" pkskew="1.5960000000" pkkurt="4.1780000000" heightdivarea="23.3108721744" baselinewidth="10.5480015278" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1141.3325368786" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0590000004" peakasymmetryvalue="1.6169999838"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="21" groupid="1"/></COMPOUND><USERDATA sampleid="21" groupid="1"/></SAMPLE><SAMPLE id="22" groupid="1" name="5-29-13 redo Dewitt dose male mouse DB005" createdate="29-May-13" createtime="17:35:44" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="25" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="22" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="247.3206787109" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="352.4147033691" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="22" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="22" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="54.3004379272" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="22" groupid="1"/></COMPOUND><USERDATA sampleid="22" groupid="1"/></SAMPLE><SAMPLE id="23" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 9" createdate="29-May-13" createtime="17:38:23" type="Analyte" text="Analyte" desc="M6 0 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="26" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:C,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="23" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="282.9920000000" height="6768.0000000000" response="0.1182295344" pkflags="bb" analconc="26.0468900475" empc="26.0470000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7300000191" endrt="0.8616999984" startht="1024.2000000000" endht="1157.0000000000" absresponse="585.3160000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="311.4682922363" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5490000000" pksigma="3.7810000000" pkskew="-0.2000000000" pkkurt="0.2230000000" heightdivarea="23.9158704133" baselinewidth="7.9019987583" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="21.7293386476" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0509999990" peaktailwidth="0.0399999991" peakasymmetryvalue="0.7839999795"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="302.3240000000" height="7060.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="911.0000000000" endht="995.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.9361000061" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="275.8876953125" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="3.8630000000" pkskew="0.8450000000" pkkurt="0.4340000000" heightdivarea="23.3524298435" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="25.5901227925" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0480000004" peakasymmetryvalue="1.2890000343"/><ISPEAK area="4950.6750000000" height="112313.0000000000" foundrt="0.7225000262" absresponse="4950.6750000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="23" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="23" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4950.6750000000" height="112313.0000000000" response="4950.6750000000" pkflags="bb" analconc="1.2157861569" empc="1.2160000000" bsanalconc="0.0000000000" conccalc="21.5786156900" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8398000002" startht="80.6000000000" endht="832.6000000000" absresponse="4950.6750000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="40.4550437927" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4950.6750000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6130000000" pksigma="3.0620000000" pkskew="1.4250000000" pkkurt="3.1860000000" heightdivarea="22.6864013493" baselinewidth="9.6660017967" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2776.2422054329" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0630000010" peakasymmetryvalue="1.7389999628"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="23" groupid="1"/></COMPOUND><USERDATA sampleid="23" groupid="1"/></SAMPLE><SAMPLE id="24" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 10" createdate="29-May-13" createtime="17:41:01" type="Analyte" text="Analyte" desc="M8 1 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="27" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="24" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="9577.9480000000" height="242450.0000000000" response="4.5727751148" pkflags="bb" analconc="1654.1471293715" empc="1654.1470000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="3059.4000000000" endht="2500.0000000000" absresponse="18221.1370000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="252.9174194336" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6090000000" pksigma="2.3380000000" pkskew="0.8590000000" pkkurt="1.8510000000" heightdivarea="25.3133552197" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="958.6132918127" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1679999828"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="8643.1890000000" height="217888.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1311.6150000000" endht="2028.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1081000566" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="236.2539062500" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6090000000" pksigma="2.3470000000" pkskew="0.9440000000" pkkurt="2.1270000000" heightdivarea="25.2092138677" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="922.2619996362" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0590000153"/><ISPEAK area="3984.7000000000" height="90414.0000000000" foundrt="0.7300000191" absresponse="3984.7000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="24" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="24" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3984.7000000000" height="90414.0000000000" response="3984.7000000000" pkflags="bb" analconc="0.9785621353" empc="0.9790000000" bsanalconc="0.0000000000" conccalc="-2.1437864700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8544999957" startht="68.2000000000" endht="543.2000000000" absresponse="3984.7000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="91.4916839600" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3984.7000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6030000000" pksigma="3.1680000000" pkskew="1.6570000000" pkkurt="4.3740000000" heightdivarea="22.6902903606" baselinewidth="10.5480015278" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="988.2209626786" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0570000000" peakasymmetryvalue="1.5230000019"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="24" groupid="1"/></COMPOUND><USERDATA sampleid="24" groupid="1"/></SAMPLE><SAMPLE id="25" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 11" createdate="29-May-13" createtime="17:43:40" type="Analyte" text="Analyte" desc="M9 1 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="28" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="25" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="8497.3400000000" height="214808.0000000000" response="3.8317584617" pkflags="db" analconc="1363.8551285139" empc="1363.8550000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8837000132" startht="1319.2000000000" endht="2181.6000000000" absresponse="16597.5300000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="288.2661743164" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6040000000" pksigma="2.3140000000" pkskew="0.9010000000" pkkurt="1.9160000000" heightdivarea="25.2794403896" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="745.1724105660" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0399999991" peakasymmetryvalue="1.1119999886"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="8100.1900000000" height="202985.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8763999939" startht="1392.9400000000" endht="2167.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0490000248" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="260.8050537109" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6030000000" pksigma="2.2850000000" pkskew="0.8230000000" pkkurt="1.6560000000" heightdivarea="25.0592887327" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="778.3016360756" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0349999666"/><ISPEAK area="4331.5700000000" height="99003.0000000000" foundrt="0.7225000262" absresponse="4331.5700000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="25" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="25" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4331.5700000000" height="99003.0000000000" response="4331.5700000000" pkflags="bb" analconc="1.0637464272" empc="1.0640000000" bsanalconc="0.0000000000" conccalc="6.3746427200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8544999957" startht="106.4000000000" endht="612.4000000000" absresponse="4331.5700000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="62.2995376587" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4331.5700000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6050000000" pksigma="3.1650000000" pkskew="1.6980000000" pkkurt="4.5330000000" heightdivarea="22.8561468474" baselinewidth="10.5480015278" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1589.1450197013" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0599999987" peakasymmetryvalue="1.6929999590"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="25" groupid="1"/></COMPOUND><USERDATA sampleid="25" groupid="1"/></SAMPLE><SAMPLE id="26" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 12" createdate="29-May-13" createtime="17:46:19" type="Analyte" text="Analyte" desc="M10 1 mg/kg 11/10/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="29" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="26" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="11698.4420000000" height="290887.0000000000" response="5.6979744019" pkflags="db" analconc="2113.4286046771" empc="2113.4290000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1347.9880000000" endht="2221.6000000000" absresponse="22972.5120000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="227.2257843018" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6100000000" pksigma="2.3600000000" pkskew="0.8460000000" pkkurt="1.6870000000" heightdivarea="24.8654478947" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1280.1672173511" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1390000582"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="11274.0700000000" height="277429.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="1633.7350000000" endht="2422.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0376000404" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="300.4327087402" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6060000000" pksigma="2.3670000000" pkskew="0.8160000000" pkkurt="1.5620000000" heightdivarea="24.6077060015" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="923.4314105255" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2209999561"/><ISPEAK area="4031.6980000000" height="92284.0000000000" foundrt="0.7225000262" absresponse="4031.6980000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="26" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="26" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4031.6980000000" height="92284.0000000000" response="4031.6980000000" pkflags="MM" analconc="0.9901038984" empc="0.9900000000" bsanalconc="0.0000000000" conccalc="-0.9896101600" modifieddate="30-May-13" modifiedtime="10:13:52" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6273000240" endrt="0.8179000020" startht="0.0000000000" endht="2250.7950000000" absresponse="4031.6980000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="59.7238616943" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4031.6980000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6570000000" pksigma="3.0230000000" pkskew="1.1280000000" pkkurt="2.1370000000" heightdivarea="22.8896112754" baselinewidth="11.4359986782" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1545.1780474663" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="26" groupid="1"/></COMPOUND><USERDATA sampleid="26" groupid="1"/></SAMPLE><SAMPLE id="27" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 13" createdate="29-May-13" createtime="17:48:57" type="Analyte" text="Analyte" desc="M1 0 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="30" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="27" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="134.0020000000" height="3686.0000000000" response="0.0567942188" pkflags="bb" analconc="5.3061004004" empc="5.3060000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8398000002" startht="1193.2000000000" endht="1046.0000000000" absresponse="230.8940000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="211.1625823975" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5950000000" pksigma="2.4380000000" pkskew="0.2170000000" pkkurt="-0.5020000000" heightdivarea="27.5070521336" baselinewidth="4.3919992447" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="17.4557440914" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0270000007" peakasymmetryvalue="0.7689999938"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="96.8920000000" height="2626.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8398000002" startht="1165.0000000000" endht="1262.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.3830000162" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="263.1391906738" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="3.1580000000" pksigma="2.6360000000" pkskew="0.2300000000" pkkurt="-0.7220000000" heightdivarea="27.1023407505" baselinewidth="4.3919992447" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="9.9795092980" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0320000015" peakasymmetryvalue="0.9010000229"/><ISPEAK area="4065.4490000000" height="90594.0000000000" foundrt="0.7225000262" absresponse="4065.4490000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="27" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="27" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4065.4490000000" height="90594.0000000000" response="4065.4490000000" pkflags="bb" analconc="0.9983924648" empc="0.9980000000" bsanalconc="0.0000000000" conccalc="-0.1607535200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6492999792" endrt="0.8471000195" startht="25.2000000000" endht="486.8000000000" absresponse="4065.4490000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="68.6996459961" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4065.4490000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6310000000" pksigma="3.2480000000" pkskew="1.4680000000" pkkurt="3.3280000000" heightdivarea="22.2838854946" baselinewidth="11.8680024147" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1318.6967514382" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0649999976" peakasymmetryvalue="1.7419999838"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="27" groupid="1"/></COMPOUND><USERDATA sampleid="27" groupid="1"/></SAMPLE><SAMPLE id="28" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 14" createdate="30-May-13" createtime="09:35:22" type="Analyte" text="Analyte" desc="M5 0 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="31" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="28" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="172.2660000000" height="4136.0000000000" response="0.0897628028" pkflags="bb" analconc="16.4314657723" empc="16.4310000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8690000176" startht="835.0000000000" endht="1012.4000000000" absresponse="319.8500000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="184.3877563477" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6060000000" pksigma="4.0910000000" pkskew="0.6530000000" pkkurt="-0.2430000000" heightdivarea="24.0093808413" baselinewidth="7.4640011787" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="22.4309904406" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0719999969" peakasymmetryvalue="2.0060000420"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="147.5840000000" height="3430.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7225000262" endrt="0.8398000002" startht="698.0000000000" endht="931.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1671999693" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="204.1398620605" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6930000000" pksigma="3.5830000000" pkskew="-0.1570000000" pkkurt="-0.1090000000" heightdivarea="23.2410017346" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="16.8022059258" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0419999994" peaktailwidth="0.0419999994" peakasymmetryvalue="0.9850000143"/><ISPEAK area="3563.2800000000" height="78226.0000000000" foundrt="0.7080000043" absresponse="3563.2800000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="28" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="28" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3563.2800000000" height="78226.0000000000" response="3563.2800000000" pkflags="bb" analconc="0.8750698636" empc="0.8750000000" bsanalconc="0.0000000000" conccalc="-12.4930136400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6492999792" endrt="0.8544999957" startht="60.8000000000" endht="356.2000000000" absresponse="3563.2800000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="60.7654037476" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3563.2800000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6240000000" pksigma="3.5980000000" pkskew="1.8140000000" pkkurt="4.8190000000" heightdivarea="21.9533688063" baselinewidth="12.3120009899" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1287.3443633318" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0659999996" peakasymmetryvalue="1.7779999971"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="28" groupid="1"/></COMPOUND><USERDATA sampleid="28" groupid="1"/></SAMPLE><SAMPLE id="29" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 15" createdate="30-May-13" createtime="08:00:04" type="Analyte" text="Analyte" desc="M6 0 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="32" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="29" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="208.8070000000" height="5314.0000000000" response="0.0848585974" pkflags="bb" analconc="14.7757990736" empc="14.7760000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8471000195" startht="1289.6000000000" endht="1355.8000000000" absresponse="363.1180000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="320.8499755859" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6250000000" pksigma="2.7800000000" pkskew="0.2100000000" pkkurt="-0.3280000000" heightdivarea="25.4493383842" baselinewidth="5.2799999714" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="16.5622577664" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0350000001" peakasymmetryvalue="0.9530000091"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="154.3110000000" height="4180.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8398000002" startht="1439.0000000000" endht="1845.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.3531999588" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="214.4960632324" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.0000000000" pksigma="2.7470000000" pkskew="0.1620000000" pkkurt="-0.5550000000" heightdivarea="27.0881531453" baselinewidth="4.8419988155" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="19.4875371464" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0340000018" peaktailwidth="0.0289999992" peakasymmetryvalue="0.8470000029"/><ISPEAK area="4279.0950000000" height="94433.0000000000" foundrt="0.7225000262" absresponse="4279.0950000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="29" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="29" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4279.0950000000" height="94433.0000000000" response="4279.0950000000" pkflags="bs" analconc="1.0508596232" empc="1.0510000000" bsanalconc="0.0000000000" conccalc="5.0859623200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8179000020" startht="102.2000000000" endht="134.2430000000" absresponse="4279.0950000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="71.8394470215" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4279.0950000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6230000000" pksigma="3.0150000000" pkskew="1.0890000000" pkkurt="1.8190000000" heightdivarea="22.0684513898" baselinewidth="9.2340016365" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1314.5006527091" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0640000030" peakasymmetryvalue="1.6809999943"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="29" groupid="1"/></COMPOUND><USERDATA sampleid="29" groupid="1"/></SAMPLE><SAMPLE id="30" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 16" createdate="30-May-13" createtime="08:02:43" type="Analyte" text="Analyte" desc="M8 1 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="33" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="30" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="2750.1100000000" height="69680.0000000000" response="1.1524066554" pkflags="bb" analconc="381.3727064570" empc="381.3730000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1791.2000000000" endht="1564.6000000000" absresponse="5379.4020000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="312.9942626953" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6020000000" pksigma="2.5770000000" pkskew="1.0870000000" pkkurt="2.4030000000" heightdivarea="25.3371683314" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="222.6238890130" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0390000008" peakasymmetryvalue="1.0800000429"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="2629.2920000000" height="65516.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1804.8000000000" endht="1752.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0460000038" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="291.1878051758" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6120000000" pksigma="2.7220000000" pkskew="1.1550000000" pkkurt="2.6270000000" heightdivarea="24.9177345080" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="224.9956860675" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0340000018" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2489999533"/><ISPEAK area="4667.9720000000" height="104320.0000000000" foundrt="0.7225000262" absresponse="4667.9720000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="30" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="30" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4667.9720000000" height="104320.0000000000" response="4667.9720000000" pkflags="bb" analconc="1.1463599890" empc="1.1460000000" bsanalconc="0.0000000000" conccalc="14.6359989000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8471000195" startht="136.0000000000" endht="440.0000000000" absresponse="4667.9720000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="73.8956222534" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4667.9720000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6020000000" pksigma="3.2070000000" pkskew="1.5020000000" pkkurt="3.5130000000" heightdivarea="22.3480346497" baselinewidth="10.5420005322" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1411.7209764097" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6469999552"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="30" groupid="1"/></COMPOUND><USERDATA sampleid="30" groupid="1"/></SAMPLE><SAMPLE id="31" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 17" createdate="30-May-13" createtime="08:05:22" type="Analyte" text="Analyte" desc="M10 1 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="34" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:D,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="31" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="3919.4800000000" height="98762.0000000000" response="1.7122424009" pkflags="bb" analconc="578.8646813037" empc="578.8650000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="2316.0000000000" endht="1639.6000000000" absresponse="7567.8580000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="323.4585876465" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6100000000" pksigma="2.5390000000" pkskew="1.0250000000" pkkurt="2.2140000000" heightdivarea="25.1977303112" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="305.3312039683" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0399999991" peakasymmetryvalue="1.1050000191"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="3648.3780000000" height="91139.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8763999939" startht="1989.8000000000" endht="1827.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0743000507" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="270.2137451172" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6040000000" pksigma="2.5010000000" pkskew="0.9600000000" pkkurt="1.8480000000" heightdivarea="24.9806900491" baselinewidth="7.0379984379" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="337.2848407859" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1890000105"/><ISPEAK area="4419.8520000000" height="98189.0000000000" foundrt="0.7225000262" absresponse="4419.8520000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="31" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="31" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4419.8520000000" height="98189.0000000000" response="4419.8520000000" pkflags="bb" analconc="1.0854267099" empc="1.0850000000" bsanalconc="0.0000000000" conccalc="8.5426709900" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8544999957" startht="36.4000000000" endht="583.6000000000" absresponse="4419.8520000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="69.6519775391" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4419.8520000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6290000000" pksigma="3.3500000000" pkskew="1.6210000000" pkkurt="4.0130000000" heightdivarea="22.2154497481" baselinewidth="11.4300012589" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1409.7087185347" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0640000030" peakasymmetryvalue="1.7189999819"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="31" groupid="1"/></COMPOUND><USERDATA sampleid="31" groupid="1"/></SAMPLE><SAMPLE id="32" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 18" createdate="30-May-13" createtime="08:08:01" type="Analyte" text="Analyte" desc="M11 1 mg/kg 11/19/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="35" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="32" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="201.7700000000" height="4735.0000000000" response="0.0795598778" pkflags="bb" analconc="12.9872288824" empc="12.9870000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7300000191" endrt="0.8690000176" startht="951.4000000000" endht="1384.0000000000" absresponse="347.2620000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="202.8825988770" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.7980000000" pksigma="4.2700000000" pkskew="-0.1100000000" pkkurt="-0.0770000000" heightdivarea="23.4673142687" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="23.3386205925" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0549999997" peaktailwidth="0.0439999998" peakasymmetryvalue="0.8000000119"><SECONDARYPEAK ion="1" foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="145.4920000000" height="3830.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7666000128" endrt="0.8690000176" startht="1381.4000000000" endht="1255.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.3868000507" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="274.4325256348" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5350000000" pksigma="3.5230000000" pkskew="0.6320000000" pkkurt="-0.2880000000" heightdivarea="26.3244714486" baselinewidth="6.1440002918" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="13.9560716833" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0329999998" peakasymmetryvalue="0.9570000172"/><ISPEAK area="4364.7880000000" height="101667.0000000000" foundrt="0.7300000191" absresponse="4364.7880000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="32" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="32" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4364.7880000000" height="101667.0000000000" response="4364.7880000000" pkflags="bb" analconc="1.0719040996" empc="1.0720000000" bsanalconc="0.0000000000" conccalc="7.1904099600" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8616999984" startht="36.4000000000" endht="594.2000000000" absresponse="4364.7880000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="56.1845970154" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4364.7880000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5990000000" pksigma="3.1770000000" pkskew="1.6720000000" pkkurt="4.4670000000" heightdivarea="23.2925402104" baselinewidth="10.9800016880" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1809.5172947875" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0599999987" peakasymmetryvalue="1.6560000181"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="32" groupid="1"/></COMPOUND><USERDATA sampleid="32" groupid="1"/></SAMPLE><SAMPLE id="33" groupid="1" name="5-29-13 redo Dewitt dose male mouse DB006" createdate="30-May-13" createtime="08:10:40" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="36" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="33" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="219.9718017578" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="294.7214660645" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="33" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="33" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="56.6423187256" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="33" groupid="1"/></COMPOUND><USERDATA sampleid="33" groupid="1"/></SAMPLE><SAMPLE id="34" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 19" createdate="30-May-13" createtime="08:13:19" type="Analyte" text="Analyte" desc="M1 0 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="37" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="34" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="54.5110000000" height="1431.0000000000" response="0.0128499066" pkflags="bbI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8544999957" startht="978.8000000000" endht="1136.8000000000" absresponse="54.5110000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="220.7081604004" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="2.5800000000" pksigma="3.5220000000" pkskew="0.1660000000" pkkurt="-0.8060000000" heightdivarea="26.2515822495" baselinewidth="5.7239985466" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="6.4836750821" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0320000015" peaktailwidth="0.0390000008" peakasymmetryvalue="1.2250000238"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="208.8447875977" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4242.1320000000" height="95125.0000000000" foundrt="0.7300000191" absresponse="4242.1320000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="34" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="34" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4242.1320000000" height="95125.0000000000" response="4242.1320000000" pkflags="bb" analconc="1.0417822542" empc="1.0420000000" bsanalconc="0.0000000000" conccalc="4.1782254200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8471000195" startht="148.8000000000" endht="884.6000000000" absresponse="4242.1320000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="59.9554939270" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4242.1320000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6210000000" pksigma="3.2140000000" pkskew="1.5810000000" pkkurt="3.7490000000" heightdivarea="22.4238661126" baselinewidth="10.1040029526" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1586.5935508065" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0590000004" peakasymmetryvalue="1.5420000553"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="34" groupid="1"/></COMPOUND><USERDATA sampleid="34" groupid="1"/></SAMPLE><SAMPLE id="35" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 20" createdate="30-May-13" createtime="08:15:57" type="Analyte" text="Analyte" desc="M2 0 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="38" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="35" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="29.7810000000" height="775.0000000000" response="0.0065566328" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:14:12" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8398000002" startht="868.6000000000" endht="1311.0000000000" absresponse="29.7810000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="251.2665100098" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="2.7800000000" pksigma="3.1260000000" pkskew="-0.1840000000" pkkurt="-0.9140000000" heightdivarea="26.0233034485" baselinewidth="4.8419988155" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3.0843744356" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0309999995" peaktailwidth="0.0320000015" peakasymmetryvalue="1.0119999647"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="281.8196411133" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4542.1180000000" height="104178.0000000000" foundrt="0.7300000191" absresponse="4542.1180000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="35" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="35" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="86" foundrt="0.7300000191" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4542.1180000000" height="104178.0000000000" response="4542.1180000000" pkflags="bb" analconc="1.1154527791" empc="1.1150000000" bsanalconc="0.0000000000" conccalc="11.5452779100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8544999957" startht="54.6000000000" endht="606.2000000000" absresponse="4542.1180000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="80.8019485474" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4542.1180000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6360000000" pksigma="3.0860000000" pkskew="1.5690000000" pkkurt="4.0120000000" heightdivarea="22.9359959385" baselinewidth="10.5480015278" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1289.3005908012" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5590000153"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="35" groupid="1"/></COMPOUND><USERDATA sampleid="35" groupid="1"/></SAMPLE><SAMPLE id="36" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 21" createdate="30-May-13" createtime="08:18:36" type="Analyte" text="Analyte" desc="M3 0 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="39" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="36" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="19.5090000000" height="608.0000000000" response="0.0045722329" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:40:50" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8251000047" startht="891.4000000000" endht="1479.2000000000" absresponse="19.5090000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="313.7887573242" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="1.8350000000" pksigma="2.9090000000" pkskew="-0.2690000000" pkkurt="-0.9210000000" heightdivarea="31.1651032857" baselinewidth="4.3919992447" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1.9376092540" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0189999994" peakasymmetryvalue="0.5529999733"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="210.1351623535" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4266.8430000000" height="93599.0000000000" foundrt="0.7225000262" absresponse="4266.8430000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="36" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="36" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4266.8430000000" height="93599.0000000000" response="4266.8430000000" pkflags="bb" analconc="1.0478507785" empc="1.0480000000" bsanalconc="0.0000000000" conccalc="4.7850778500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8544999957" startht="49.8000000000" endht="733.4000000000" absresponse="4266.8430000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="65.7969207764" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4266.8430000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6030000000" pksigma="3.5010000000" pkskew="1.7140000000" pkkurt="4.1680000000" heightdivarea="21.9363590364" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1422.5437740184" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0659999996" peakasymmetryvalue="1.7039999962"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="36" groupid="1"/></COMPOUND><USERDATA sampleid="36" groupid="1"/></SAMPLE><SAMPLE id="37" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 22" createdate="30-May-13" createtime="08:21:15" type="Analyte" text="Analyte" desc="M5 0 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="40" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="37" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="96" foundrt="0.8032000065" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="29197.6170000000" height="708303.0000000000" response="13.2596042771" pkflags="db" analconc="6276.6762193679" empc="6276.6760000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="2084.1530000000" endht="4761.0000000000" absresponse="55888.1580000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="271.5143432617" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6110000000" pksigma="2.3980000000" pkskew="0.8390000000" pkkurt="1.5370000000" heightdivarea="24.2589318163" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2608.7130112211" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0430000015" peakasymmetryvalue="1.1640000343"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="26690.5410000000" height="646266.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1954.9250000000" endht="3751.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0938999653" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="199.5797424316" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6230000000" pksigma="2.4440000000" pkskew="0.8000000000" pkkurt="1.5270000000" heightdivarea="24.2132971377" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3238.1342521341" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0460000001" peakasymmetryvalue="1.2619999647"/><ISPEAK area="4214.9190000000" height="94559.0000000000" foundrt="0.7225000262" absresponse="4214.9190000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="37" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="37" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4214.9190000000" height="94559.0000000000" response="4214.9190000000" pkflags="bb" analconc="1.0350992890" empc="1.0350000000" bsanalconc="0.0000000000" conccalc="3.5099289000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8398000002" startht="68.0000000000" endht="901.4000000000" absresponse="4214.9190000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="54.7917709351" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4214.9190000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6150000000" pksigma="3.1530000000" pkskew="1.5200000000" pkkurt="3.7980000000" heightdivarea="22.4343575760" baselinewidth="10.1039993763" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1725.7883508105" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0579999983" peakasymmetryvalue="1.4900000095"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="37" groupid="1"/></COMPOUND><USERDATA sampleid="37" groupid="1"/></SAMPLE><SAMPLE id="38" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 23" createdate="30-May-13" createtime="08:23:52" type="Analyte" text="Analyte" desc="M6 0 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="41" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="38" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="30326.2090000000" height="734291.0000000000" response="14.6261461170" pkflags="db" analconc="7553.0435603306" empc="7553.0440000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="2369.0790000000" endht="4155.0000000000" absresponse="57855.7540000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="292.8353271484" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6060000000" pksigma="2.4650000000" pkskew="0.8390000000" pkkurt="1.6180000000" heightdivarea="24.2130824858" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2507.5219139383" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0469999984" peakasymmetryvalue="1.2760000229"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="27529.5450000000" height="665434.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="3001.0850000000" endht="4328.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1016000509" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="266.9944763184" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6130000000" pksigma="2.4350000000" pkskew="0.8120000000" pkkurt="1.3740000000" heightdivarea="24.1716308788" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2492.3137331371" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0450000018" peakasymmetryvalue="1.2209999561"/><ISPEAK area="3955.6390000000" height="91187.0000000000" foundrt="0.7153000236" absresponse="3955.6390000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="38" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="38" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3955.6390000000" height="91187.0000000000" response="3955.6390000000" pkflags="bb" analconc="0.9714253385" empc="0.9710000000" bsanalconc="0.0000000000" conccalc="-2.8574661500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8179000020" startht="55.0000000000" endht="1321.8000000000" absresponse="3955.6390000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="63.7642707825" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3955.6390000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6630000000" pksigma="2.9780000000" pkskew="1.2340000000" pkkurt="2.4540000000" heightdivarea="23.0524069562" baselinewidth="9.2340016365" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1430.0641861189" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0590000004" peakasymmetryvalue="1.6089999676"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="38" groupid="1"/></COMPOUND><USERDATA sampleid="38" groupid="1"/></SAMPLE><SAMPLE id="39" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 24" createdate="30-May-13" createtime="08:26:31" type="Analyte" text="Analyte" desc="M7 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="42" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:E,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="39" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="52.0370000000" height="1232.0000000000" response="0.0127016478" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:14:26" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7372000217" endrt="0.8324000239" startht="851.2000000000" endht="1234.8000000000" absresponse="52.0370000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="234.7955474854" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="2.4200000000" pksigma="3.4960000000" pkskew="-0.1580000000" pkkurt="-0.7740000000" heightdivarea="23.6754616907" baselinewidth="5.7120001316" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="5.2471182405" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0489999987" peaktailwidth="0.0289999992" peakasymmetryvalue="0.5899999738"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="298.2713317871" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="4096.8700000000" height="90677.0000000000" foundrt="0.7153000236" absresponse="4096.8700000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="39" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="39" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4096.8700000000" height="90677.0000000000" response="4096.8700000000" pkflags="bb" analconc="1.0061088301" empc="1.0060000000" bsanalconc="0.0000000000" conccalc="0.6108830100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8398000002" startht="69.6000000000" endht="687.6000000000" absresponse="4096.8700000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="41.9864654541" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4096.8700000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6450000000" pksigma="3.3280000000" pkskew="1.6130000000" pkkurt="3.9110000000" heightdivarea="22.1332383014" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2159.6721471858" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0610000007" peakasymmetryvalue="1.5570000410"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="39" groupid="1"/></COMPOUND><USERDATA sampleid="39" groupid="1"/></SAMPLE><SAMPLE id="40" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 25" createdate="30-May-13" createtime="08:29:09" type="Analyte" text="Analyte" desc="M8 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="43" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="40" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="11.9050000000" height="420.0000000000" response="0.0030224427" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:40:56" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8104000092" startht="1202.0000000000" endht="1364.0000000000" absresponse="11.9050000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="345.5269165039" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="1.2150000000" pksigma="2.4800000000" pkskew="-0.1260000000" pkkurt="-1.1260000000" heightdivarea="35.2792944141" baselinewidth="3.5099995136" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1.2155348250" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0140000004" peakasymmetryvalue="0.3869999945"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="291.2482604980" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="3938.8670000000" height="86718.0000000000" foundrt="0.7153000236" absresponse="3938.8670000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="40" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="40" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3938.8670000000" height="86718.0000000000" response="3938.8670000000" pkflags="bb" analconc="0.9673064729" empc="0.9670000000" bsanalconc="0.0000000000" conccalc="-3.2693527100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8398000002" startht="68.8000000000" endht="651.2000000000" absresponse="3938.8670000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="47.9917335510" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3938.8670000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6370000000" pksigma="3.3820000000" pkskew="1.6110000000" pkkurt="3.8500000000" heightdivarea="22.0159756600" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1806.9361863705" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0619999990" peakasymmetryvalue="1.5839999914"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="40" groupid="1"/></COMPOUND><USERDATA sampleid="40" groupid="1"/></SAMPLE><SAMPLE id="41" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 26" createdate="30-May-13" createtime="08:31:48" type="Analyte" text="Analyte" desc="M9 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="44" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="41" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="37.9120000000" height="1000.0000000000" response="0.0236064851" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:40:59" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8324000239" startht="982.2000000000" endht="1261.4000000000" absresponse="91.9110000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="285.2182922363" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="0.8030000000" pksigma="3.3800000000" pkskew="-0.0980000000" pkkurt="-0.9250000000" heightdivarea="26.3768727580" baselinewidth="5.2680015564" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3.5060864861" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0410000011" peaktailwidth="0.0329999998" peakasymmetryvalue="0.8109999895"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="53.9990000000" height="1122.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8616999984" startht="921.6000000000" endht="1025.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.7020999789" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="196.0501098633" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="1.3280000000" pksigma="4.2210000000" pkskew="0.1880000000" pkkurt="-1.0160000000" heightdivarea="20.7781625586" baselinewidth="6.5879988670" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="5.7230266322" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0399999991" peaktailwidth="0.0619999990" peakasymmetryvalue="1.5670000315"/><ISPEAK area="3893.4640000000" height="85901.0000000000" foundrt="0.7080000043" absresponse="3893.4640000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="41" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="41" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3893.4640000000" height="85901.0000000000" response="3893.4640000000" pkflags="bb" analconc="0.9561564097" empc="0.9560000000" bsanalconc="0.0000000000" conccalc="-4.3843590300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8544999957" startht="64.4000000000" endht="494.6000000000" absresponse="3893.4640000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="84.5488128662" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3893.4640000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6500000000" pksigma="3.5510000000" pkskew="1.8210000000" pkkurt="4.8640000000" heightdivarea="22.0628725474" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1015.9929759857" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0659999996" peakasymmetryvalue="1.7979999781"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="41" groupid="1"/></COMPOUND><USERDATA sampleid="41" groupid="1"/></SAMPLE><SAMPLE id="42" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 27" createdate="30-May-13" createtime="08:34:27" type="Analyte" text="Analyte" desc="M10 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="45" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="42" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="22213.1930000000" height="521818.0000000000" response="10.7895217841" pkflags="MM" analconc="4602.1972417870" empc="4602.1970000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:26:42" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="3443.0490000000" endht="3167.6050000000" absresponse="42773.3220000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="273.8789672852" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6330000000" pksigma="2.5300000000" pkskew="0.9380000000" pkkurt="1.8530000000" heightdivarea="23.4913548899" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1905.2868687675" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0350000001" peaktailwidth="0.0489999987" peakasymmetryvalue="1.3899999857"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="20560.1290000000" height="500210.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8690000176" startht="7239.8000000000" endht="4354.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0803999901" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="338.1163330078" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6200000000" pksigma="2.4820000000" pkskew="0.7890000000" pkkurt="1.3110000000" heightdivarea="24.3291275069" baselinewidth="7.4640011787" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1479.4020612676" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0469999984" peakasymmetryvalue="1.2840000391"/><ISPEAK area="3964.3390000000" height="88432.0000000000" foundrt="0.7080000043" absresponse="3964.3390000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="42" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="42" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3964.3390000000" height="88432.0000000000" response="3964.3390000000" pkflags="bb" analconc="0.9735618835" empc="0.9740000000" bsanalconc="0.0000000000" conccalc="-2.6438116500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8544999957" startht="14.6000000000" endht="415.4000000000" absresponse="3964.3390000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="71.8954925537" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3964.3390000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6160000000" pksigma="3.3730000000" pkskew="1.8160000000" pkkurt="5.2270000000" heightdivarea="22.3068713347" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1230.0075687490" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6679999828"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="42" groupid="1"/></COMPOUND><USERDATA sampleid="42" groupid="1"/></SAMPLE><SAMPLE id="43" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 28" createdate="30-May-13" createtime="08:37:05" type="Analyte" text="Analyte" desc="M11 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="46" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="43" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="28275.3870000000" height="668807.0000000000" response="13.5813120755" pkflags="db" analconc="6542.7403979393" empc="6542.7400000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="3926.6940000000" endht="4423.2000000000" absresponse="52451.4890000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="267.7685241699" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6200000000" pksigma="2.4660000000" pkskew="0.8460000000" pkkurt="1.4460000000" heightdivarea="23.6533278926" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2497.7058153989" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0450000018" peakasymmetryvalue="1.1549999714"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="24176.1020000000" height="580537.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8763999939" startht="8103.6000000000" endht="3928.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1696000099" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="329.5098876953" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6280000000" pksigma="2.5290000000" pkskew="0.8550000000" pkkurt="1.5430000000" heightdivarea="24.0128454124" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1761.8196651410" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0469999984" peakasymmetryvalue="1.3009999990"/><ISPEAK area="3862.0340000000" height="89247.0000000000" foundrt="0.7080000043" absresponse="3862.0340000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="43" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="43" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3862.0340000000" height="89247.0000000000" response="3862.0340000000" pkflags="bb" analconc="0.9484378342" empc="0.9480000000" bsanalconc="0.0000000000" conccalc="-5.1562165800" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6639999747" endrt="0.8032000065" startht="153.6000000000" endht="1502.6000000000" absresponse="3862.0340000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="74.0186843872" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3862.0340000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6130000000" pksigma="2.8830000000" pkskew="1.1620000000" pkkurt="2.0890000000" heightdivarea="23.1088074315" baselinewidth="8.3520019054" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1205.7361021594" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0570000000" peakasymmetryvalue="1.5750000477"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="43" groupid="1"/></COMPOUND><USERDATA sampleid="43" groupid="1"/></SAMPLE><SAMPLE id="44" groupid="1" name="5-29-13 redo Dewitt dose male mouse DB007" createdate="30-May-13" createtime="08:39:44" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="47" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="44" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="289.4273071289" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="280.6461791992" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="44" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="44" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="70.4918289185" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="44" groupid="1"/></COMPOUND><USERDATA sampleid="44" groupid="1"/></SAMPLE><SAMPLE id="45" groupid="1" name="5-29-13 redo Dewitt dose male mouse sample 29" createdate="30-May-13" createtime="08:42:23" type="Analyte" text="Analyte" desc="M12 1 mg/kg 12/3/12" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="48" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="45" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="22528.0630000000" height="551195.0000000000" response="11.0555740046" pkflags="db" analconc="4760.2799180332" empc="4760.2800000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="2134.0820000000" endht="3908.6000000000" absresponse="44710.6760000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="202.9284362793" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6120000000" pksigma="2.4540000000" pkskew="0.8870000000" pkkurt="1.8480000000" heightdivarea="24.4670391769" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2716.2038505110" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0450000018" peakasymmetryvalue="1.2369999886"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="22182.6130000000" height="540020.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="2556.0210000000" endht="3618.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0155999660" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="274.5494995117" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6140000000" pksigma="2.3800000000" pkskew="0.8570000000" pkkurt="1.6550000000" heightdivarea="24.3442916306" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1966.9312854710" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1360000372"/><ISPEAK area="4044.1750000000" height="90782.0000000000" foundrt="0.7153000236" absresponse="4044.1750000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="45" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="45" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4044.1750000000" height="90782.0000000000" response="4044.1750000000" pkflags="MM" analconc="0.9931679985" empc="0.9930000000" bsanalconc="0.0000000000" conccalc="-0.6832001500" modifieddate="30-May-13" modifiedtime="10:14:42" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6492999792" endrt="0.9203000069" startht="56.2000000000" endht="57.2000000000" absresponse="4044.1750000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="60.0558242798" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4044.1750000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6250000000" pksigma="3.5120000000" pkskew="2.2880000000" pkkurt="8.8330000000" heightdivarea="22.4475943796" baselinewidth="16.2600016594" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1511.6269086087" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0610000007" peakasymmetryvalue="1.7000000477"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="45" groupid="1"/></COMPOUND><USERDATA sampleid="45" groupid="1"/></SAMPLE><SAMPLE id="46" groupid="1" name="5-29-13 redo Dewitt dose male mouse rep 1" createdate="30-May-13" createtime="08:45:02" type="Analyte" text="Analyte" desc="rep M7 1 mg/kg 12/3/21" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="49" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="46" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="92" foundrt="0.7738000154" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="49.1910000000" height="1004.0000000000" response="0.0125607341" pkflags="MMI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="30-May-13" modifiedtime="10:23:49" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7372000217" endrt="0.8398000002" startht="980.2760000000" endht="1193.3790000000" absresponse="49.1910000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="287.1192321777" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.7420000000" pksigma="3.9550000000" pkskew="0.0250000000" pkkurt="-0.9740000000" heightdivarea="20.4102376451" baselinewidth="6.1559987068" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="3.4968051161" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0379999988" peaktailwidth="0.0630000010" peakasymmetryvalue="1.6360000372"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="263.3665466309" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="3916.2520000000" height="87180.0000000000" foundrt="0.7080000043" absresponse="3916.2520000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="46" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="46" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3916.2520000000" height="87180.0000000000" response="3916.2520000000" pkflags="bb" analconc="0.9617526839" empc="0.9620000000" bsanalconc="0.0000000000" conccalc="-3.8247316100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8616999984" startht="67.0000000000" endht="429.2000000000" absresponse="3916.2520000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="56.0966873169" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3916.2520000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6130000000" pksigma="3.5820000000" pkskew="1.9570000000" pkkurt="5.8050000000" heightdivarea="22.2610802369" baselinewidth="12.2999989986" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1554.1024643312" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6469999552"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="46" groupid="1"/></COMPOUND><USERDATA sampleid="46" groupid="1"/></SAMPLE><SAMPLE id="47" groupid="1" name="5-29-13 redo Dewitt dose male mouse rep 2" createdate="30-May-13" createtime="08:47:41" type="Analyte" text="Analyte" desc="rep M3 0 mg/kg 12/3/21" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="50" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:F,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="47" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="57.8700000000" height="1175.0000000000" response="0.0155336981" pkflags="bbI" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7225000262" endrt="0.8324000239" startht="845.2000000000" endht="848.6000000000" absresponse="57.8700000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="263.7274780273" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="2.4020000000" pksigma="4.0950000000" pkskew="-0.2360000000" pkkurt="-0.8910000000" heightdivarea="20.3041299464" baselinewidth="6.5939998627" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="4.4553567523" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0680000037" peaktailwidth="0.0329999998" peakasymmetryvalue="0.4920000136"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="230.9771118164" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="3725.4490000000" height="84405.0000000000" foundrt="0.7225000262" absresponse="3725.4490000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="47" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="47" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3725.4490000000" height="84405.0000000000" response="3725.4490000000" pkflags="bb" analconc="0.9148953067" empc="0.9150000000" bsanalconc="0.0000000000" conccalc="-8.5104693300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8616999984" startht="96.0000000000" endht="568.8000000000" absresponse="3725.4490000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="48.9034194946" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3725.4490000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6280000000" pksigma="3.4390000000" pkskew="1.8810000000" pkkurt="5.2820000000" heightdivarea="22.6563294787" baselinewidth="10.9800016880" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1725.9529266511" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0599999987" peakasymmetryvalue="1.6000000238"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="47" groupid="1"/></COMPOUND><USERDATA sampleid="47" groupid="1"/></SAMPLE><SAMPLE id="48" groupid="1" name="5-29-13 redo Dewitt dose male mouse rep 3" createdate="30-May-13" createtime="08:50:20" type="Analyte" text="Analyte" desc="rep M10 1 mg/kg 12/3/21" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="51" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="2:A,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="48" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="23685.5430000000" height="579384.0000000000" response="12.3087309080" pkflags="db" analconc="5568.4863570209" empc="5568.4860000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7591000199" endrt="0.8837000132" startht="1910.9220000000" endht="4060.0000000000" absresponse="46051.2950000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="226.1680603027" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6300000000" pksigma="2.3550000000" pkskew="0.8950000000" pkkurt="1.8850000000" heightdivarea="24.4615037958" baselinewidth="7.4759995937" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2561.7410310920" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0340000018" peaktailwidth="0.0439999998" peakasymmetryvalue="1.2690000534"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="22365.7520000000" height="557860.0000000000" response="0.0000000000" pkflags="db" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1811.6190000000" endht="3336.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0590000153" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="245.7289581299" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6050000000" pksigma="2.3910000000" pkskew="0.9290000000" pkkurt="2.1150000000" heightdivarea="24.9425997391" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="2270.2249024518" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1629999876"/><ISPEAK area="3741.3520000000" height="87732.0000000000" foundrt="0.7225000262" absresponse="3741.3520000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="48" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="48" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3741.3520000000" height="87732.0000000000" response="3741.3520000000" pkflags="bb" analconc="0.9188007635" empc="0.9190000000" bsanalconc="0.0000000000" conccalc="-8.1199236500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6786999702" endrt="0.8544999957" startht="59.2000000000" endht="485.8000000000" absresponse="3741.3520000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="73.7073059082" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3741.3520000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6190000000" pksigma="3.1200000000" pkskew="1.7190000000" pkkurt="4.9410000000" heightdivarea="23.4492771597" baselinewidth="10.5480015278" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1190.2754946608" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5429999828"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="48" groupid="1"/></COMPOUND><USERDATA sampleid="48" groupid="1"/></SAMPLE><SAMPLE id="49" groupid="1" name="5-29-13 redo Dewitt dose male mouse new QCL" createdate="30-May-13" createtime="08:52:58" type="QC" text="QC" desc="100 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="52" stdconc="100.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="2:A,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="49" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="100.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="663.7620000000" height="16408.0000000000" response="0.3301329723" pkflags="bb" analconc="97.8941165005" empc="97.8940000000" bsanalconc="0.0000000000" conccalc="-2.1058834995" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7300000191" endrt="0.8690000176" startht="906.0000000000" endht="1147.6000000000" absresponse="1268.4960000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="272.3435974121" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0033013297" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6020000000" pksigma="3.2590000000" pkskew="0.7530000000" pkkurt="1.4500000000" heightdivarea="24.7197037492" baselinewidth="8.3399999142" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="60.2474233135" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1640000343"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="604.7340000000" height="14638.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8616999984" startht="927.8000000000" endht="1321.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0975999832" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="201.7449645996" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6460000000" pksigma="3.1270000000" pkskew="0.9710000000" pkkurt="1.0300000000" heightdivarea="24.2056838213" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="72.5569534241" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0430000015" peakasymmetryvalue="1.1770000458"/><ISPEAK area="3842.3790000000" height="85583.0000000000" foundrt="0.7080000043" absresponse="3842.3790000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="49" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="49" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3842.3790000000" height="85583.0000000000" response="3842.3790000000" pkflags="bb" analconc="0.9436109617" empc="0.9440000000" bsanalconc="0.0000000000" conccalc="-5.6389038300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6492999792" endrt="0.8324000239" startht="154.2000000000" endht="713.4000000000" absresponse="3842.3790000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="64.4648437500" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3842.3790000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6320000000" pksigma="3.3350000000" pkskew="1.5890000000" pkkurt="3.9550000000" heightdivarea="22.2734404909" baselinewidth="10.9860026836" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1327.5918317882" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0579999983" peakasymmetryvalue="1.5579999685"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="49" groupid="1"/></COMPOUND><USERDATA sampleid="49" groupid="1"/></SAMPLE><SAMPLE id="50" groupid="1" name="5-29-13 redo Dewitt dose male mouse new QCH" createdate="30-May-13" createtime="08:55:37" type="QC" text="QC" desc="1000 ng/mL" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="53" stdconc="1000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="2:A,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="50" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="1000.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5216.1570000000" height="126042.0000000000" response="2.4615711092" pkflags="bb" analconc="849.3235914193" empc="849.3240000000" bsanalconc="0.0000000000" conccalc="-15.0676408581" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8763999939" startht="1393.2000000000" endht="2031.0000000000" absresponse="10236.7290000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="241.7450408936" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0024615711" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6470000000" pksigma="2.6160000000" pkskew="1.0380000000" pkkurt="2.1590000000" heightdivarea="24.1637665431" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="521.3840148866" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0469999984" peakasymmetryvalue="1.3079999685"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5020.5720000000" height="122992.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8763999939" startht="1180.0000000000" endht="1394.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0390000343" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="241.2664947510" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6040000000" pksigma="2.5600000000" pkskew="1.1090000000" pkkurt="2.4590000000" heightdivarea="24.4976070456" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="509.7765445092" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0439999998" peakasymmetryvalue="1.2009999752"/><ISPEAK area="4158.6160000000" height="93372.0000000000" foundrt="0.7080000043" absresponse="4158.6160000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="50" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="50" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="4158.6160000000" height="93372.0000000000" response="4158.6160000000" pkflags="bb" analconc="1.0212724052" empc="1.0210000000" bsanalconc="0.0000000000" conccalc="2.1272405200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6420000196" endrt="0.8398000002" startht="59.0000000000" endht="653.2000000000" absresponse="4158.6160000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="72.8263854980" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="4158.6160000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6270000000" pksigma="3.3180000000" pkskew="1.6870000000" pkkurt="4.5050000000" heightdivarea="22.4526621357" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1282.1177291918" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0619999990" peakasymmetryvalue="1.6740000248"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="50" groupid="1"/></COMPOUND><USERDATA sampleid="50" groupid="1"/></SAMPLE><SAMPLE id="51" groupid="1" name="5-29-13 redo Dewitt dose male mouse DB008" createdate="30-May-13" createtime="08:58:16" type="Blank" text="Blank" desc="75:25 2mM:ACN DB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="54" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="2:A,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="51" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="285.5563659668" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="288.3575134277" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="0.0000000000" height="0.0000000000" foundrt="0.0000000000" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="51" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="51" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="64.7864990234" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="51" groupid="1"/></COMPOUND><USERDATA sampleid="51" groupid="1"/></SAMPLE><SAMPLE id="52" groupid="1" name="5-29-13 redo Dewitt dose male mouse MBb" createdate="30-May-13" createtime="09:00:55" type="Blank" text="Blank" desc="MB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="55" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="52" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="205.4085083008" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="302.3159179688" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="84.8860000000" height="2386.0000000000" foundrt="0.7957999706" absresponse="0.0000000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="52" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="52" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="84.8860000000" height="2386.0000000000" response="0.0000000000" pkflags="MM-" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="30-May-13" modifiedtime="10:14:58" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7957999706" endrt="0.8984000087" startht="156.8530000000" endht="236.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="65.4673690796" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="28.1082864077" baselinewidth="6.1560022831" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="36.4456374763" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0080000004" peaktailwidth="0.0810000002" peakasymmetryvalue="9.8750000000"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="52" groupid="1"/></COMPOUND><USERDATA sampleid="52" groupid="1"/></SAMPLE><SAMPLE id="53" groupid="1" name="5-29-13 redo Dewitt dose male mouse MtxBb" createdate="30-May-13" createtime="09:03:33" type="Blank" text="Blank" desc="MtxB" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="56" stdconc="0.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="53" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="0.0000000000"><PEAK foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="" empc="" bsanalconc="" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="297.0628356934" detectionthreshold="" detectionflag="0" quanthreshold="" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 168.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"><SECONDARYPEAK ion="1" foundscan="0" foundrt="0.0000000000" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="0.0000000000" height="0.0000000000" response="0.0000000000" pkflags="" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="NaN" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.0000000000" endrt="0.0000000000" startht="0.0000000000" endht="0.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="214.9870605469" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="0.0000000000" pksigma="0.0000000000" pkskew="0.0000000000" pkkurt="0.0000000000" heightdivarea="0.0000000000" baselinewidth="0.0000000000" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="0.0000000000" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0000000000" peaktailwidth="0.0000000000" peakasymmetryvalue="0.0000000000"/><ISPEAK area="3606.8500000000" height="84254.0000000000" foundrt="0.7225000262" absresponse="3606.8500000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="53" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="53" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3606.8500000000" height="84254.0000000000" response="3606.8500000000" pkflags="bb" analconc="0.8857697789" empc="0.8860000000" bsanalconc="0.0000000000" conccalc="-11.4230221100" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8471000195" startht="70.6000000000" endht="550.2000000000" absresponse="3606.8500000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="58.4645118713" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3606.8500000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6080000000" pksigma="3.0740000000" pkskew="1.6540000000" pkkurt="4.6020000000" heightdivarea="23.3594410635" baselinewidth="10.5420005322" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1441.1135456910" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0529999994" peakasymmetryvalue="1.4229999781"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="53" groupid="1"/></COMPOUND><USERDATA sampleid="53" groupid="1"/></SAMPLE><SAMPLE id="54" groupid="1" name="5-29-13 redo Dewitt dose male mouse std1b" createdate="30-May-13" createtime="09:06:12" type="Standard" text="Standard" desc="10 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="57" stdconc="10.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,4" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="54" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="10.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="118.8780000000" height="3148.0000000000" response="0.0643977112" pkflags="bb" analconc="7.8709102269" empc="7.8710000000" bsanalconc="0.0000000000" conccalc="-21.2908977310" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8471000195" startht="991.4000000000" endht="1180.8000000000" absresponse="244.9110000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="284.8983459473" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0064397711" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5510000000" pksigma="3.3320000000" pkskew="0.1110000000" pkkurt="-0.3240000000" heightdivarea="26.4809300291" baselinewidth="6.1500012875" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="11.0495552002" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0299999993" peakasymmetryvalue="0.8429999948"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="126.0330000000" height="2967.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8398000002" startht="797.8000000000" endht="1010.6000000000" absresponse="0.0000000000" rrtref="0" ionratio="0.9431999922" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="180.5023345947" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6120000000" pksigma="2.9080000000" pkskew="0.1260000000" pkkurt="-0.5480000000" heightdivarea="23.5414534289" baselinewidth="5.2739989758" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="16.4374605274" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0399999991" peakasymmetryvalue="1.0190000534"/><ISPEAK area="3803.1010000000" height="88937.0000000000" foundrt="0.7153000236" absresponse="3803.1010000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="54" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="54" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3803.1010000000" height="88937.0000000000" response="3803.1010000000" pkflags="bb" analconc="0.9339650753" empc="0.9340000000" bsanalconc="0.0000000000" conccalc="-6.6034924700" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8544999957" startht="67.8000000000" endht="477.2000000000" absresponse="3803.1010000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="81.9041595459" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3803.1010000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.5970000000" pksigma="3.2680000000" pkskew="1.8720000000" pkkurt="5.4990000000" heightdivarea="23.3853899752" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1085.8667068082" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0560000017" peakasymmetryvalue="1.5349999666"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="54" groupid="1"/></COMPOUND><USERDATA sampleid="54" groupid="1"/></SAMPLE><SAMPLE id="55" groupid="1" name="5-29-13 redo Dewitt dose male mouse std2b" createdate="30-May-13" createtime="09:08:50" type="Standard" text="Standard" desc="25 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="58" stdconc="25.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,5" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="55" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="25.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="222.9840000000" height="5535.0000000000" response="0.1118188945" pkflags="bb" analconc="23.8807723801" empc="23.8810000000" bsanalconc="0.0000000000" conccalc="-4.4769104796" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8544999957" startht="972.2000000000" endht="1150.4000000000" absresponse="442.0410000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="274.6779479980" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0044727558" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5550000000" pksigma="3.2670000000" pkskew="0.6610000000" pkkurt="-0.0880000000" heightdivarea="24.8224087827" baselinewidth="6.1559987068" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="20.1508713762" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0340000018" peaktailwidth="0.0529999994" peakasymmetryvalue="1.5449999571"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="219.0570000000" height="5480.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8544999957" startht="788.4000000000" endht="1065.0000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0178999901" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="222.8354644775" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5960000000" pksigma="3.3280000000" pkskew="0.6930000000" pkkurt="0.1540000000" heightdivarea="25.0163199533" baselinewidth="6.5939998627" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="24.5921357843" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1349999905"/><ISPEAK area="3953.1870000000" height="90322.0000000000" foundrt="0.7080000043" absresponse="3953.1870000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="55" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="55" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3953.1870000000" height="90322.0000000000" response="3953.1870000000" pkflags="bb" analconc="0.9708231767" empc="0.9710000000" bsanalconc="0.0000000000" conccalc="-2.9176823300" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8471000195" startht="98.4000000000" endht="413.0000000000" absresponse="3953.1870000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="47.5532455444" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3953.1870000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6220000000" pksigma="3.2400000000" pkskew="1.7470000000" pkkurt="4.9550000000" heightdivarea="22.8478946227" baselinewidth="11.4240002632" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1899.3866552306" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0599999987" peakasymmetryvalue="1.6399999857"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="55" groupid="1"/></COMPOUND><USERDATA sampleid="55" groupid="1"/></SAMPLE><SAMPLE id="56" groupid="1" name="5-29-13 redo Dewitt dose male mouse std3b" createdate="30-May-13" createtime="09:11:30" type="Standard" text="Standard" desc="50 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="59" stdconc="50.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,6" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="56" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="50.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="429.3610000000" height="11101.0000000000" response="0.2210769839" pkflags="bb" analconc="60.8580607168" empc="60.8580000000" bsanalconc="0.0000000000" conccalc="21.7161214336" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8471000195" startht="1040.2000000000" endht="1294.6000000000" absresponse="818.1900000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="190.1873779297" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0044215397" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5960000000" pksigma="2.6890000000" pkskew="0.1470000000" pkkurt="0.3510000000" heightdivarea="25.8547003570" baselinewidth="6.1500012875" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="58.3687525473" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0340000018" peakasymmetryvalue="0.9530000091"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="388.8290000000" height="9624.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8544999957" startht="816.2000000000" endht="1156.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1042000055" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="220.6740112305" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5940000000" pksigma="2.9610000000" pkskew="0.5190000000" pkkurt="0.4110000000" heightdivarea="24.7512402624" baselinewidth="6.5939998627" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="43.6118414957" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0290000439"/><ISPEAK area="3700.9280000000" height="86591.0000000000" foundrt="0.7225000262" absresponse="3700.9280000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="56" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="56" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3700.9280000000" height="86591.0000000000" response="3700.9280000000" pkflags="bb" analconc="0.9088734425" empc="0.9090000000" bsanalconc="0.0000000000" conccalc="-9.1126557500" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8471000195" startht="140.4000000000" endht="722.8000000000" absresponse="3700.9280000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="70.6774444580" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3700.9280000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6070000000" pksigma="3.1500000000" pkskew="1.7720000000" pkkurt="5.0420000000" heightdivarea="23.3971047262" baselinewidth="10.5420005322" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1225.1574836078" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0500000007" peakasymmetryvalue="1.3470000029"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="56" groupid="1"/></COMPOUND><USERDATA sampleid="56" groupid="1"/></SAMPLE><SAMPLE id="57" groupid="1" name="5-29-13 redo Dewitt dose male mouse std4b" createdate="30-May-13" createtime="09:14:08" type="Standard" text="Standard" desc="100 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="60" stdconc="100.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,7" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="57" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="100.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="807.1030000000" height="19567.0000000000" response="0.4036180626" pkflags="bb" analconc="122.9223969411" empc="122.9220000000" bsanalconc="0.0000000000" conccalc="22.9223969411" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="871.0000000000" endht="1038.2000000000" absresponse="1536.5110000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="252.6051177979" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0040361806" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6120000000" pksigma="3.2720000000" pkskew="1.2910000000" pkkurt="2.0640000000" heightdivarea="24.2434980418" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="77.4608217386" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0460000001" peakasymmetryvalue="1.2580000162"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="729.4080000000" height="18505.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8616999984" startht="909.8000000000" endht="1063.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1065000296" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="267.0103454590" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.5710000000" pksigma="2.8420000000" pkskew="0.8980000000" pkkurt="1.3080000000" heightdivarea="25.3698890059" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="69.3044307635" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1260000467"/><ISPEAK area="3806.8440000000" height="85724.0000000000" foundrt="0.7080000043" absresponse="3806.8440000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="57" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="57" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3806.8440000000" height="85724.0000000000" response="3806.8440000000" pkflags="bb" analconc="0.9348842808" empc="0.9350000000" bsanalconc="0.0000000000" conccalc="-6.5115719200" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8544999957" startht="73.0000000000" endht="436.4000000000" absresponse="3806.8440000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="76.6778717041" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3806.8440000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6190000000" pksigma="3.5370000000" pkskew="1.8560000000" pkkurt="5.0650000000" heightdivarea="22.5183905618" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1117.9757353048" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0630000010" peakasymmetryvalue="1.7159999609"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="57" groupid="1"/></COMPOUND><USERDATA sampleid="57" groupid="1"/></SAMPLE><SAMPLE id="58" groupid="1" name="5-29-13 redo Dewitt dose male mouse std5b" createdate="30-May-13" createtime="09:16:47" type="Standard" text="Standard" desc="250 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="61" stdconc="250.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:A,8" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="58" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="250.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="1702.3030000000" height="42216.0000000000" response="0.8542308274" pkflags="bb" analconc="277.6957653441" empc="277.6960000000" bsanalconc="0.0000000000" conccalc="11.0783061376" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7225000262" endrt="0.8690000176" startht="747.0000000000" endht="1346.4000000000" absresponse="3164.2760000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="239.6226654053" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0034169233" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.5980000000" pksigma="2.7690000000" pkskew="0.4280000000" pkkurt="1.9250000000" heightdivarea="24.7993453574" baselinewidth="8.7899994850" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="176.1769903052" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0419999994" peakasymmetryvalue="1.1579999924"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="1461.9730000000" height="37096.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8690000176" startht="1057.6000000000" endht="1136.8000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1643999815" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="173.5471191406" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6030000000" pksigma="2.6150000000" pkskew="0.9400000000" pkkurt="1.9660000000" heightdivarea="25.3739296143" baselinewidth="7.4640011787" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="213.7517475582" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0370000005" peakasymmetryvalue="1.0260000229"/><ISPEAK area="3704.2400000000" height="84440.0000000000" foundrt="0.7225000262" absresponse="3704.2400000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="58" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="58" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="85" foundrt="0.7225000262" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3704.2400000000" height="84440.0000000000" response="3704.2400000000" pkflags="bb" analconc="0.9096868031" empc="0.9100000000" bsanalconc="0.0000000000" conccalc="-9.0313196900" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6714000106" endrt="0.8398000002" startht="106.6000000000" endht="612.8000000000" absresponse="3704.2400000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="50.5407829285" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3704.2400000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6040000000" pksigma="3.1100000000" pkskew="1.6150000000" pkkurt="4.1240000000" heightdivarea="22.7954992117" baselinewidth="10.1039993763" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1670.7299552425" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0390000008" peaktailwidth="0.0549999997" peakasymmetryvalue="1.4149999619"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="58" groupid="1"/></COMPOUND><USERDATA sampleid="58" groupid="1"/></SAMPLE><SAMPLE id="59" groupid="1" name="5-29-13 redo Dewitt dose male mouse std6b" createdate="30-May-13" createtime="09:19:26" type="Standard" text="Standard" desc="500 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="62" stdconc="500.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,1" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="59" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="500.0000000000"><PEAK foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="3055.7310000000" height="75658.0000000000" response="1.5791432118" pkflags="bb" analconc="531.5680809428" empc="531.5680000000" bsanalconc="0.0000000000" conccalc="6.3136161886" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8616999984" startht="907.2000000000" endht="1637.4000000000" absresponse="5687.1690000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="186.1867980957" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0031582864" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6050000000" pksigma="2.4110000000" pkskew="0.8060000000" pkkurt="1.3600000000" heightdivarea="24.7593783615" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="406.3553419137" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0329999998" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2979999781"><SECONDARYPEAK ion="1" foundscan="94" foundrt="0.7885000110" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="2631.4380000000" height="64442.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8690000176" startht="1081.8000000000" endht="1199.4000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1612000465" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="236.6389770508" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6170000000" pksigma="2.6030000000" pkskew="0.9370000000" pkkurt="1.7410000000" heightdivarea="24.4892716454" baselinewidth="7.4640011787" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="272.3220020773" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0450000018" peakasymmetryvalue="1.2439999580"/><ISPEAK area="3601.4270000000" height="82177.0000000000" foundrt="0.7080000043" absresponse="3601.4270000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="59" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="59" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="83" foundrt="0.7080000043" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3601.4270000000" height="82177.0000000000" response="3601.4270000000" pkflags="bb" analconc="0.8844379992" empc="0.8840000000" bsanalconc="0.0000000000" conccalc="-11.5562000800" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8398000002" startht="58.0000000000" endht="726.8000000000" absresponse="3601.4270000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="71.7138214111" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3601.4270000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6310000000" pksigma="3.3340000000" pkskew="1.7610000000" pkkurt="4.7520000000" heightdivarea="22.8178996825" baselinewidth="10.9859991074" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1145.9018412766" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0590000004" peakasymmetryvalue="1.6130000353"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="59" groupid="1"/></COMPOUND><USERDATA sampleid="59" groupid="1"/></SAMPLE><SAMPLE id="60" groupid="1" name="5-29-13 redo Dewitt dose male mouse std7b" createdate="30-May-13" createtime="09:22:04" type="Standard" text="Standard" desc="1000 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="63" stdconc="1000.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,2" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="60" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="1000.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5529.2450000000" height="138605.0000000000" response="2.9758527756" pkflags="bb" analconc="1039.2725964818" empc="1039.2730000000" bsanalconc="0.0000000000" conccalc="3.9272596482" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8763999939" startht="1192.4000000000" endht="1632.2000000000" absresponse="10558.1590000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="202.6273193359" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0029758528" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6110000000" pksigma="2.3870000000" pkskew="0.9530000000" pkkurt="2.0100000000" heightdivarea="25.0676177308" baselinewidth="7.4699985981" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="684.0390548236" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0410000011" peakasymmetryvalue="1.1649999619"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="5028.9140000000" height="126069.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7445999980" endrt="0.8763999939" startht="980.2000000000" endht="2020.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.0994999409" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="200.2324676514" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6160000000" pksigma="2.4750000000" pkskew="1.0830000000" pkkurt="2.5550000000" heightdivarea="25.0688319586" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="629.6131765179" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0379999988" peakasymmetryvalue="1.0369999409"/><ISPEAK area="3547.9440000000" height="80898.0000000000" foundrt="0.7153000236" absresponse="3547.9440000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="60" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="60" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3547.9440000000" height="80898.0000000000" response="3547.9440000000" pkflags="bb" analconc="0.8713036506" empc="0.8710000000" bsanalconc="0.0000000000" conccalc="-12.8696349400" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6567000151" endrt="0.8544999957" startht="86.4000000000" endht="404.2000000000" absresponse="3547.9440000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="62.7022018433" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3547.9440000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6080000000" pksigma="3.3140000000" pkskew="1.7950000000" pkkurt="4.9690000000" heightdivarea="22.8013745426" baselinewidth="11.8679988384" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1290.1939265582" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0610000007" peakasymmetryvalue="1.6909999847"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="60" groupid="1"/></COMPOUND><USERDATA sampleid="60" groupid="1"/></SAMPLE><SAMPLE id="61" groupid="1" name="5-29-13 redo Dewitt dose male mouse std8b" createdate="30-May-13" createtime="09:24:44" type="Standard" text="Standard" desc="2500 ng/mL std" dilutionfac="0.0000000000" extractvolume="0.0000000000" initamount="0.0000000000" injectvolume="40.0000000000" job="5-28-13 redo Dewitt dosed male mouse serum U2M3O-h" sampleid="" samplenumber="64" stdconc="2500.0000000000" stockdilutionfac="0.0000000000" subjecttext="" subjecttime="0.0000000000" userdilutionfac="0.0000000000" vial="1:B,3" inletmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\7-12-12 PFOA in mouse seruum grad MeOH 2 min" msmethodname="D:\Masslynx\new MJS.PRO\ACQUDB\4-22-13 U2M3O-hexane with PFHxA IS.EXP" prerunmethodname="" postrunmethodname="" switchmethodname="" hplcmethodname="" tunemethodname="D:\Masslynx\new MJS.PRO\ACQUDB\U2M3Ohex MRM.IPR" fractionlynxname="" instrument="" lab="" conditions="" submitter="" task="" user="" reinjections="0"><COMPOUND id="1" sampleid="61" groupid="1" name="U2M3O-hex" type="" cas="" stdconc="2500.0000000000"><PEAK foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="12724.7940000000" height="314711.0000000000" response="6.9667676211" pkflags="bb" analconc="2662.2803847886" empc="2662.2800000000" bsanalconc="0.0000000000" conccalc="6.4912153915" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8837000132" startht="1945.4000000000" endht="2338.2000000000" absresponse="24291.1680000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="215.5644836426" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0027867070" chromtrace="329.16 &gt; 168.9" peaks="1" pkwidth="2.6090000000" pksigma="2.4040000000" pkskew="0.9190000000" pkkurt="1.9700000000" heightdivarea="24.7321096121" baselinewidth="7.9079997540" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1459.9390153798" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0430000015" peakasymmetryvalue="1.2079999447"><SECONDARYPEAK ion="1" foundscan="95" foundrt="0.7957999706" foundrrt="0.0000000000" predrt="0.7950000167" predrrt="1.0000000000" area="11566.3740000000" height="288751.0000000000" response="0.0000000000" pkflags="bb" analconc="0.0000000000" empc="0.0000000000" bsanalconc="0.0000000000" conccalc="-100.0000000000" modifieddate="" modifiedtime="" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.7519000173" endrt="0.8690000176" startht="1780.6000000000" endht="2787.2000000000" absresponse="0.0000000000" rrtref="0" ionratio="1.1002000570" ionratiopred="0.0000000000" ionratiowin="20" ionratioflag="0" chromnoise="183.4594726563" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="0.0000000000" chromtrace="329.16 &gt; 284.9" peaks="0" pkwidth="2.6050000000" pksigma="2.3090000000" pkskew="0.8080000000" pkkurt="1.4200000000" heightdivarea="24.9646950721" baselinewidth="7.0260000229" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1573.9225444141" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0370000005" peaktailwidth="0.0399999991" peakasymmetryvalue="1.0870000124"/><ISPEAK area="3486.7200000000" height="79591.0000000000" foundrt="0.7153000236" absresponse="3486.7200000000"/></PEAK><METHOD rref="2.0000000000" predrt="0.7950000167" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="329.16 &gt; 168.9" secondarytrace="329.16 &gt; 284.9" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="U2M3O-hex"/><USERDATA sampleid="61" groupid="1"/></COMPOUND><COMPOUND id="2" sampleid="61" groupid="1" name="13C-PFHxA" type="" cas="" stdconc="1.0000000000"><PEAK foundscan="84" foundrt="0.7153000236" foundrrt="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" area="3486.7200000000" height="79591.0000000000" response="3486.7200000000" pkflags="MM" analconc="0.8562682683" empc="0.8560000000" bsanalconc="0.0000000000" conccalc="-14.3731731700" modifieddate="30-May-13" modifiedtime="10:15:56" modifiedtext="" modifieduser="" peakmass="0.0000000000" startrt="0.6492999792" endrt="0.8179000020" startht="0.0000000000" endht="963.4700000000" absresponse="3486.7200000000" rrtref="0" quanratio="0.0000000000" quanratiopred="1.0000000000" quanratiowin="0.0000000000" ionratio="0.0000000000" ionratiopred="0.0000000000" ionratiowin="0" ionratioflag="0" chromnoise="69.9970779419" detectionthreshold="0.0000000000" detectionflag="0" quanthreshold="0.0000000000" quanflag="0" snlodflag="0" snloqflag="0" rrf="3486.7200000000" chromtrace="314.75 &gt; 269.75" peaks="0" pkwidth="2.6300000000" pksigma="2.9070000000" pkskew="1.3010000000" pkkurt="2.8810000000" heightdivarea="22.8268974853" baselinewidth="10.1160013676" replimflag="0" maxreplimflag="0" recovlimflag="0" matrixblankflag="0" solventblankflag="0" devflag="0" devflagmidconc="0" devflaglowconc="0" qcsignoiseflag="0" qcionratioflag="0" qcrettimeflag="0" qcpeakshapeflag="0" signoiseflag="0" signoise="1137.0617508644" cdflag="0" stddevflag="0" rtflag="0" peakasymmetry="0" peakfrontwidth="0.0359999985" peaktailwidth="0.0540000014" peakasymmetryvalue="1.4989999533"><ISPEAK area="" height="" foundrt="" absresponse=""/></PEAK><METHOD rref="0.0000000000" predrt="0.7649999857" predrrt="1.0000000000" userfactor="0.0000000000" userrf="0.0000000000" quantrace="314.75 &gt; 269.75" secondarytrace="" useabsmasswin="1" chromasswinabs="0.0199999996" chromasswinppm="10.0000000000" stockconcfactor="1.0000000000" calibref="13C-PFHxA"/><USERDATA sampleid="61" groupid="1"/></COMPOUND><USERDATA sampleid="61" groupid="1"/></SAMPLE></SAMPLELISTDATA><CALIBRATIONDATA filename="" modifieddate="30 May 2013" modifiedtime="10:16:34" count="2"><COMPOUND id="1" name="U2M3O-hex"><RESPONSE type="Internal Std" ref="2" rah="Area * ( IS Conc. / IS Area )"/><CURVE type="2nd Order" origin="Exclude" weighting="1/x" axistrans="None"><CALIBRATIONCURVE curve="-0.000000 * x^2 + 0.002966 * x + 0.041058"/><DETERMINATION rsquared="0.9919589659"/></CURVE></COMPOUND><COMPOUND id="2" name="13C-PFHxA"><RESPONSE type="External Std" ref="" rah="Area"/><CURVE type="RF" origin="" weighting="" axistrans=""><RESPONSEFACTOR cc="4071.9948750000" stddev="411.2253754100" percrelsd="10.0988677060"/></CURVE></COMPOUND></CALIBRATIONDATA></GROUP></GROUPDATA></QUANDATASET>
